Zobrazeno 1 - 10
of 23
pro vyhledávání: '"Jacco D. van Beek"'
Publikováno v:
JOURNAL OF MAGNETIC RESONANCE
Journal of magnetic resonance (San Diego Calif. : 1997)
Journal of magnetic resonance (San Diego Calif. : 1997)
Spin diffusion type polarization transfer among heteronuclei e.g. 13C or 15N plays an important role in many solid state NMR experiments for structure determination of proteins. In such experiments chemical shift compensation is provided by the proto
Autor:
Renana Gershoni-Poranne, Louis Bertschi, Amnon Stanger, Malte Standera, Gunnar Jeschke, A. Dieter Schlüter, Rolf Häfliger, Jacco D. van Beek
Publikováno v:
Chemistry-A European Journal
A chain of circumstantial evidence for the existence of the first fully conjugated, double-stranded cycles is presented. The products have the structure of the belt-region of fullerene C(84) (D(2)) and carry either four hexyl chains or four phenyl gr
Publikováno v:
Journal of Magnetic Resonance. 207:197-205
Zero-quantum coherence generation and reconversion in magic-angle spinning solid-state NMR is analyzed. Two methods are discussed based on implementations using symmetry-based pulse sequences that utilize either isotropic J couplings or dipolar coupl
Autor:
Jacco D. van Beek
Publikováno v:
Journal of Magnetic Resonance. 187:19-26
matNMR (matnmr.sourceforge.net) is a toolbox for processing, analyzing and visualizing magnetic-resonance data within the Matlab ® environment ( www.mathworks.com ) that aims for control, flexibility and extendability. Processing can be done using e
Publikováno v:
Journal of the Mechanics and Physics of Solids. 54:589-610
In this study, spatial orientational distribution functions of labeled chain segments of cross-linked and linear PMMA were obtained by solid-state NMR as a function of finite deformation (far) below and (far) above the glass transition temperature T
Publikováno v:
Journal of Magnetic Resonance. 179:38-48
We have performed magic-angle-spinning solid-state NMR experiments in which protons are recoupled to oxygen-17 nuclei by applying a symmetry-based recoupling sequence at the proton Larmor frequency. Two-dimensional quadrupole-dipole correlation spect
Publikováno v:
Macromolecules. 38:8372-8380
The orientational distribution function for polymer chain segments in plain-strain compressed glassy poly(methyl methacrylate) is evaluated, as a function of two polar angles, from a series of one-dimensional deuterium NMR spectra. The experimental d
Publikováno v:
Analytical Biochemistry. 311:19-26
Silk fibroins from moth larvae and spiders are composed of highly repetitive Ala- and Gly-rich blocks that determine their structure, properties, and function. To investigate the metabolic integration of isotopically labeled amino acids in the excret
Publikováno v:
Journal of the American Chemical Society. 123:910-913
It is shown that bicellar nematic liquid-crystalline phases can be oriented with the director (the normal to the bicellar plane) at an arbitrary angle to the applied magnetic field by sample rotation around one axis (variable-angle sample spinning) o
Publikováno v:
Journal of Magnetic Resonance. 140:300-303
Through-bond connectivity can be probed by J couplings. For effective two-spin systems, the INADEQUATE experiment is highly valuable in liquid-state spectroscopy. It is the purpose of this Communication to show that in-phase INADEQUATE-CR spectra, wh