Zobrazeno 1 - 10
of 116
pro vyhledávání: '"J. Pielaszek"'
Publikováno v:
Solid State Phenomena. 130:63-68
Laboratory prepared and commercial Li-Mn spinels were studied. Making use of the dedicated XRD-impedance spectroscopy experimental set-up, direct correlations of the degree of phase transformation (expressed as change of the FWHM of the selected refl
Autor:
J. Pielaszek, M. Marzantowicz, J.R. Dygas, Monika Kopec, D. Lisovytskiy, Franciszek Krok, Zbigniew Kaszkur
Publikováno v:
Journal of Power Sources. 159:412-419
Phase transition in lithium manganese oxide spinel synthesized by sol–gel technique and in samples prepared from commercially available powders of LiMn2O4 (Alfa-Aesar and Sigma–Aldrich) was investigated. In addition to the standard impedance meas
Autor:
Alain Celzard, J. Pielaszek, Bogusław Mierzwa, G. Furdin, Jean-François Marêché, S. Puricelli, Ghouti Medjahdi
Publikováno v:
Applied Catalysis A: General. 296:232-237
Molybdenum carbide is a promising catalyst in many reactions. Its formation was investigated by XRD for two different active carbons:commercial one (NC100) and made out of expanded graphite. They were impregnated by MoCl 5 from vapor phase and carbon
Publikováno v:
Solid State Ionics. 176:2153-2161
Electrical conductivity and dielectric properties of lithium manganese spinels, Li 1+ d Mn 2− d O 4 , d = 0 and d = 0.005, obtained by sol–gel method, were studied by impedance spectroscopy. Parameters of relaxation function were obtained by fitt
Publikováno v:
Solid State Ionics. 176:2059-2064
For the purpose of simultaneous measurement of electric properties and X-ray diffraction pattern during phase transition, an experimental setup was developed combining impedance analyzer and X-ray diffractometer equipped with position sensitive detec
Autor:
T. Mounis, Marie-Laure Fontaine, Ch. Laberty-Robert, D. Lisovytskiy, B. Mierzwa, J. Pielaszek
Publikováno v:
Solid State Ionics. 176:1213-1223
The formation of the perovskite and derived perovskite oxides via polymeric route has been studied by both in situ X-ray diffraction and thermogravimetric analyses. The dried gel of La1 − xSrxMnO3 and LaMn1 − yCuyO3 oxides have been synthesized f
Publikováno v:
Journal of Applied Crystallography. 38:266-273
Model powder diffraction patterns were calculatedviathe Debye formula from atom positions of a range of energy-relaxed closed-shell cubooctahedral clusters. The energy relaxation employed the Sutton–Chen potential scheme with parameters for palladi
Autor:
Dmitry V. Kazachkin, Wojciech Juszczyk, Maciej Skotak, Julie L. d'Itri, Leszek Kȩpiński, J. Pielaszek, Zbigniew Karpiński, Vladimir I. Kovalchuk
Publikováno v:
Journal of Catalysis. 227:11-25
The effect of catalyst pretreatment on the performance of chlorine-free γ -alumina-supported palladium catalysts with metal loadings in the range of 0.3 to 2.77 wt% has been investigated in the hydroconversion of n- hexane (nH) and 2,2-dimethylbutan
Autor:
Zbigniew Kaszkur, V. N. Baumer, Franciszek Krok, J. Pielaszek, D. Lisovytskiy, J.R. Dygas, Janina Molenda, Monika Kopec, J. Marzec
Publikováno v:
Materials Science Forum. :311-314
Lithium-manganese spinels obtained by sol-gel method were studied by XRD, impedance spectroscopy, electric conductivity and thermogravimetric analysis (TGA). Heating of low-temperature spinels up to 630° C leads to the formation of spinels with latt
Publikováno v:
Journal of Catalysis. 220:299-308
This work provides evidence that reduction of Pd/SiO 2 catalysts in dihydrogen at temperatures as low as 450 and 500 °C may already lead to a considerable interaction between palladium and silica, identified by the formation of palladium silicides (