Zobrazeno 1 - 10
of 26
pro vyhledávání: '"J. Mitchell Wells"'
Publikováno v:
The Analyst. 146:7104-7108
Microwave radiation is used to lyse and extract dipicolinic acid (DPA) and lipids from Bacillus subtilis spores in one minute. Molecular analysis is by nESI-MS with DPA being confirmed by MS/MS at levels as low as 105–106 spores.
Publikováno v:
The Analyst. 146(23)
Spore lysis of Bacillus species is achieved by brief (1 min) microwave irradiation while tandem mass spectrometry (MS/MS) allows identification of the characteristic spore marker, dipicolinic acid. This rapid measurement, made on 10
Publikováno v:
Journal of the American Society for Mass Spectrometry. 31(5)
Two experiments are described that extend the capabilities of quadrupole ion trap mass spectrometers operated in the precursor and neutral loss scan mode. The first experiment, a triple resonance precursor ion scan, is used to enhance sensitivity, se
Publikováno v:
The Analyst. 143:5438-5452
A new set of operations for tandem mass spectrometry in a linear ion trap is described. Logical MS/MS operations categorize compounds in mixtures based on characteristic structural features as revealed by MS/MS behavior recorded in multiple fragmenta
Autor:
Adam D. Keil, Dina R. Justes, Garth E. Patterson, Dennis J. Barket, Michael J. Roth, John W. Grossenbacher, J. Mitchell Wells
Publikováno v:
Journal of the American Society for Mass Spectrometry. 19:1419-1424
A recently developed prototype mobile laboratory mass spectrometer, incorporating an atmospheric pressure ionization (API) interface, is described. This system takes advantage of the small size, lower voltage requirements, and tandem MS abilities of
Publikováno v:
International Journal of Mass Spectrometry. 222:243-258
The performance characteristics of a new ion trap system adapted for ion/ion reaction experiments are described. Significantly improved mass analysis figures of merit over previously used ion/ion reaction instrumentation have been realized. For examp
Publikováno v:
International Journal of Mass Spectrometry. 219:171-187
The dissociation behavior of bovine ferri-, ferro-, and apo-cytochrome c ions formed by electrospray ionization has been studied as a function of precursor ion charge state under quadrupole ion trap collisional activation conditions. Tandem mass spec
Publikováno v:
International Journal of Mass Spectrometry. 212:359-376
The dissociation of the multiply protonated ions of apomyoglobin ranging in charge from [M + 2H] 2+ to [M + 21H] 21+ have been studied using collisional activation and ion/ion reactions in a quadrupole ion trap. A variety of collisional activation co
Publikováno v:
Analytical Chemistry. 73:3274-3281
One of the major factors governing the "top-down" sequence analysis of intact multiply protonated proteins by tandem mass spectrometry is the effect of the precursor ion charge state on the formation of product ions. To more fully understand this eff
Publikováno v:
Rapid Communications in Mass Spectrometry. 15:2334-2340
The dissociation of holomyoglobin ions ranging in charge state from +10 to +2 has been studied using collisional activation in a quadrupole ion trap. Collisional activation times and amplitudes were varied to investigate the effects of these variable