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pro vyhledávání: '"J L, Kacprzak"'
Autor:
J. L. Kacprzak
Publikováno v:
International Journal of Environmental Analytical Chemistry. 38:561-564
Graphite-furnace atomic absorption spectrometry for tributyltin in oysters is described. Tributyltin is extracted by n-hexane after digestion with hydrochloric acid. The 3[sgrave] detection limit for tributyltin is better than 0.01 mg Sn/kg. Typical
Autor:
J, Ziaziaris, J L, Kacprzak
Publikováno v:
Journal of AOAC International. 78(3)
Samples of raw noodles in a mixture of nitric acid and hydrogen peroxide were microwave digested in sealed tetrafluoromethaxil (PTFE TFM) vessels. The digests were diluted to volume with distilled water and quantitated by inductively coupled plasma a
Autor:
J L, Kacprzak
Publikováno v:
Journal - Association of Official Analytical Chemists. 61(6)
A gas-liquid chromatographic (GLC) procedure with p-toluenesulfonamide (p-TS) as an internal standard is used to determine o-toluenesulfonamide (o-TS), a major impurity in artificial sweetening substances containing saccharin. Although p-TS can itsel
Autor:
J L, Kacprzak, R, Chvojka
Publikováno v:
Journal - Association of Official Analytical Chemists. 59(1)
A method for the concurrent determination of methyl mercury and inorganic mercury by flameless atomic absorption spectroscopy (AAS) is described. Fifty-seven samples of juvenile black marlin fish were analyzed for inorganic and methyl mercury, and to
Autor:
R, Chvojka, J L, Kacprzak
Publikováno v:
Journal - Association of Official Analytical Chemists. 62(5)
Background correction is used with a previously published flameless atomic absorption method for the concurrent determination of inorganic and methyl mercury. The use of background correction simplifies the procedure, but, more importantly, eliminate
Publikováno v:
Journal - Association of Official Analytical Chemists. 67(1)
A method is described for determining naphthalene in bran and wheat germ products. The method involves distilling the naphthalene from a water-cereal mixture and then extracting the distillate with hexane. A 10 microL aliquot of the hexane extract is
Autor:
J L, Kacprzak
Publikováno v:
Journal - Association of Official Analytical Chemists. 60(5)
A method is described for determining dimethylpolysiloxane in instant coffee. The siloxane is extracted with chloroform in a Soxhlet apparatus and then converted to silica which is estimated by a heteropoly blue method. The method is interference-fre
Autor:
Kacprzak, J. L.
Publikováno v:
International Journal of Environmental Analytical Chemistry; Apr1990, Vol. 38 Issue 4, p561-564, 4p