Zobrazeno 1 - 10
of 54
pro vyhledávání: '"Jérôme Hirschinger"'
Autor:
Jérôme Hirschinger, Jésus Raya
Publikováno v:
Journal of Magnetic Resonance Open, Vol 16, Iss , Pp 100128- (2023)
In this work, several exact and approximate analytical solutions to the quantum master equation are derived using both classical and non-classical coupling models to describe the kinetics of Hartmann-Hahn cross-polarization (HHCP) and multiple-contac
Externí odkaz:
https://doaj.org/article/57a1ecc9944144db98ff66a2b327016b
Autor:
Vytautas, Klimavicius, Arūnas, Maršalka, Agne, Kizalaite, Aleksej, Zarkov, Aivaras, Kareiva, Kęstutis, Aidas, Jérôme, Hirschinger, Vytautas, Balevicius
Publikováno v:
Physical chemistry chemical physics : PCCP. 24(31)
The solid-state
Publikováno v:
Physical chemistry chemical physics : PCCP. 22(21)
Hartmann-Hahn cross-polarization (HHCP) is the most widely used solid-state NMR technique to enhance the magnetization of dilute spins from abundant spins. Furthermore, as the kinetics of CP depends on dipolar interactions, it contains valuable infor
Autor:
Jésus Raya, Jérôme Hirschinger
Publikováno v:
Journal of magnetic resonance (San Diego, Calif. : 1997). 281
Multiple-contact cross-polarization (MC-CP) is applied to powder samples of ferrocene and l-alanine under magic-angle spinning (MAS) conditions. The method is described analytically through the density matrix formalism. The combination of a two-step
Autor:
Jérôme Hirschinger, Camille Loupiac, Chloé Roullier-Gall, Régis D. Gougeon, Jésus Raya, Lucie Huault, Philippe Cayot, Cyrielle Maissiat, Ali Assifaoui, Maguy Jaber, Jean-François Lambert, Philippe Jeandet
Publikováno v:
RSC Advances
RSC Advances, Royal Society of Chemistry, 2014, 4 (105), pp.61096-61103. ⟨10.1039/C4RA11607K⟩
RSC Advances, 2014, 4 (105), pp.61096-61103. ⟨10.1039/C4RA11607K⟩
RSC Advances, Royal Society of Chemistry, 2014, 4 (105), pp.61096-61103. ⟨10.1039/C4RA11607K⟩
RSC Advances, 2014, 4 (105), pp.61096-61103. ⟨10.1039/C4RA11607K⟩
International audience; In this work, the adsorption of a small globular protein (betalactoglobulin, BLG), on a natural montmorillonite clay (Mt) was investigated in acidic buffer (pH = 3). The combination of different characterization techniques suc
Publikováno v:
Chemical Physics Letters. 508:155-164
We present a new simple and robust cross-polarization (CP) scheme, called ROtor-Directed Exchange of Orientations CP (RODEO-CP), which permits to obtain undistorted chemical shift powder spectra with short contact times, i.e., when a (quasi-)equilibr
Autor:
Jérôme Hirschinger
Publikováno v:
Solid State Nuclear Magnetic Resonance. 34:210-223
Using the Anderson-Weiss (AW) formalism, analytical expressions of the NMR signal are obtained for the following magic-angle spinning (MAS) experiments: total suppression of sidebands (TOSS); phase adjusted spinning sidebands (PASS); rotational-echo
Publikováno v:
Macromolecular Chemistry and Physics. 208:2204-2214
Gel networks prepared from aqueous melamine-formaldehyde resins via a sol-gel route were characterised by 13 C CPMAS (where MAS stands for magic angle spinning)-NMR and T 2 relaxation. We show that within the aqueous networks, the type and amount of
Publikováno v:
Magnetic Resonance in Chemistry. 44:174-177
The REDOR and CPMAS techniques are applied for measuring 13C15N dipolar coupling constants in glycine. It is shown that the selective CP or SPECIFIC CP technique removes the coherent evolution of the spin system under homonuclear 13C13C J couplings.
Autor:
Jérôme Hirschinger
Publikováno v:
Concepts in Magnetic Resonance Part A. :307-320
A simple analytical method based on the memory-function approach and the Anderson-Weiss theory is presented for studying in a uniform way the spin dynamics in several NMR experiments performed under the conditions of magic-angle spinning (MAS). A ser