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Monatshefte für Chemie Chemical Monthly. 123:321-324
The microcristalline phase (NH3OH)2TiF6 has been isolated from aqueous solution. It crystallizes in the tetragonal system with cell parameters:a=9.654±0.005 A,c=11.546±0.010 A. The hydroxylammonium fluorotitanate was characterized by vibrational sp