Výsledky vyhledávání - "High performance liquid chromatography/quantitative analysis"

Dissertation/ Thesis

Determinação da isotretinoína em medicamentos por cromatografia líquida de alta eficiência e caracterização por análise térmica e difração à laser

Autor: Guimarães, Carla Aiolfi

A isotretinoína (ácido-13-cis-retinóico) é uma substância derivada da vitamina A. É indicada no tratamento de formas graves de acne nódulo císticas e resistentes a terapias anteriores. É uma substância termo e fotossensível, que requer cui

Externí odkaz: http://www.teses.usp.br/teses/disponiveis/9/9139/tde-16102017-141429/

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Development and validation of a new and economical stability indicating RP-HPLC method for cefixime trihydrate

Autor: M. Ajitha, Puvvadi Sathesh Babu, Bellamkonda Swathi, Ceema Mathew

Publikováno v: Brazilian Journal of Pharmaceutical Sciences, Volume: 52, Issue: 1, Pages: 87-94, Published: MAR 2016
Brazilian Journal of Pharmaceutical Sciences; Vol. 52 No. 1 (2016); 87-94
Brazilian Journal of Pharmaceutical Sciences; Vol. 52 Núm. 1 (2016); 87-94
Brazilian Journal of Pharmaceutical Sciences; v. 52 n. 1 (2016); 87-94
Brazilian Journal of Pharmaceutical Sciences
Universidade de São Paulo (USP)
instacron:USP
Brazilian Journal of Pharmaceutical Sciences, Vol 52, Iss 1, Pp 87-94

The present work describes the development of a new high performance liquid chromatographic (HPLC) method for the determination of Cefixime trihydrate under different stress conditons as specified by ICH. For the analysis, a Phenomenex (250 x 4.6 mm,

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::d63c35eaa2494921776fe4c3ebe089fb
https://doi.org/10.1590/s1984-82502016000100010

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Validation of high performance liquid chromatography method for determination of meloxicam loaded PEGylated nanocapsules

Autor: Luciane Varini Laporta, Cristiane Luchese, Alexandre Machado Rubim, Francine R. Ianiski

Publikováno v: Brazilian Journal of Pharmaceutical Sciences; Vol. 51 No. 4 (2015); 823-832
Brazilian Journal of Pharmaceutical Sciences; Vol. 51 Núm. 4 (2015); 823-832
Brazilian Journal of Pharmaceutical Sciences; v. 51 n. 4 (2015); 823-832
Brazilian Journal of Pharmaceutical Sciences
Universidade de São Paulo (USP)
instacron:USP
Brazilian Journal of Pharmaceutical Sciences, Vol 51, Iss 4, Pp 823-832 (2015)
Brazilian Journal of Pharmaceutical Sciences, Volume: 51, Issue: 4, Pages: 823-832, Published: DEC 2015

A method to ensure that an analytical method will produce reliable and interpretable information about the sample must first be validated, making sure that the results can be trusted and traced. In this study, we propose to validate an analytical hig

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::67ce908e2d6a3ce754581831beef415d
https://doi.org/10.1590/s1984-82502015000400008

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Akademický článek

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Stability indicating RP-LC-PDA method for the quantitative analysis of saxagliptin in pharmaceutical dosage form

Autor: Laís E. Scheeren, Clarice Madalena Bueno Rolim, Andréa Inês Horn Adams, Ana Isa Pedroso Marcolino

Publikováno v: Brazilian Journal of Pharmaceutical Sciences; Vol. 51 No. 2 (2015); 461-466
Brazilian Journal of Pharmaceutical Sciences; Vol. 51 Núm. 2 (2015); 461-466
Brazilian Journal of Pharmaceutical Sciences; v. 51 n. 2 (2015); 461-466
Brazilian Journal of Pharmaceutical Sciences
Universidade de São Paulo (USP)
instacron:USP
Brazilian Journal of Pharmaceutical Sciences, Volume: 51, Issue: 2, Pages: 461-466, Published: JUN 2015
Brazilian Journal of Pharmaceutical Sciences, Vol 51, Iss 2, Pp 461-466 (2015)

Saxagliptin is a potent and selective inhibitor of the enzyme dipeptidyl peptidase 4. It is effective in the treatment of type 2 diabetes mellitus because it stimulates the pancreas to produce insulin. In the present study, a liquid chromatography me

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::f3af180a738b4fee5ca56aa0fe55c379
https://doi.org/10.1590/s1984-82502015000200023

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Development of alternative methods for the determination of raloxifene hydrochloride in tablet dosage form

Autor: Leonardo Zanchetti Meneghini, Fernanda Rodrigues Salazar, Ana Maria Bergold, Cristiane Franco Codevilla

Publikováno v: Brazilian Journal of Pharmaceutical Sciences, Vol 51, Iss 2, Pp 349-360 (2015)
Brazilian Journal of Pharmaceutical Sciences, Volume: 51, Issue: 2, Pages: 349-360, Published: JUN 2015
Brazilian Journal of Pharmaceutical Sciences; Vol. 51 No. 2 (2015); 349-360
Brazilian Journal of Pharmaceutical Sciences; Vol. 51 Núm. 2 (2015); 349-360
Brazilian Journal of Pharmaceutical Sciences; v. 51 n. 2 (2015); 349-360
Brazilian Journal of Pharmaceutical Sciences
Universidade de São Paulo (USP)
instacron:USP
Repositório Institucional da UFRGS
Universidade Federal do Rio Grande do Sul (UFRGS)
instacron:UFRGS

Three methods are proposed for the quantitative determination of raloxifene hydrochloride in pharmaceutical dosage form: ultraviolet method (UV) high performance liquid chromatography (HPLC) and micellar capillary electrophoresis (MEKC). These method

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::a2f8332f54df6fefc9ace1168c06c2c4
http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1984-82502015000200349&lng=en&tlng=en

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Pharmacokinetic-pharmacodynamic correlation of imipenem in pediatric burn patients using a bioanalytical liquid chromatographic method

Autor: Carlindo Vieira da Silva Junior, Silvia Regina Cavani Jorge Santos, Cristina Sanches-Giraud, David de Souza Gomez

Publikováno v: Brazilian Journal of Pharmaceutical Sciences, Vol 51, Iss 2, Pp 305-315 (2015)
Brazilian Journal of Pharmaceutical Sciences, Volume: 51, Issue: 2, Pages: 305-315, Published: JUN 2015
Brazilian Journal of Pharmaceutical Sciences; Vol. 51 No. 2 (2015); 305-315
Brazilian Journal of Pharmaceutical Sciences; Vol. 51 Núm. 2 (2015); 305-315
Brazilian Journal of Pharmaceutical Sciences; v. 51 n. 2 (2015); 305-315
Brazilian Journal of Pharmaceutical Sciences
Universidade de São Paulo (USP)
instacron:USP

A bioanalytical method was developed and applied to quantify the free imipenem concentrations for pharmacokinetics and PK/PD correlation studies of the dose adjustments required to maintain antimicrobial effectiveness in pediatric burn patients. A re

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::c222a7f2dbfc84f5a36ebf82916efca4
http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1984-82502015000200305&lng=en&tlng=en

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Quantification and stress degradation studies of cefepime/tazobactam in dry injection form by an RP-HPLC method

Autor: Sunitha Gurrala, Panikumar Anumolu Durga, Ramakrishna Kommana, Venkat Raj Yeradesi, Gouthami Kannabattula

Publikováno v: Brazilian Journal of Pharmaceutical Sciences, Volume: 50, Issue: 4, Pages: 895-901, Published: DEC 2014
Brazilian Journal of Pharmaceutical Sciences; Vol. 50 No. 4 (2014); 895-901
Brazilian Journal of Pharmaceutical Sciences; Vol. 50 Núm. 4 (2014); 895-901
Brazilian Journal of Pharmaceutical Sciences; v. 50 n. 4 (2014); 895-901
Brazilian Journal of Pharmaceutical Sciences
Universidade de São Paulo (USP)
instacron:USP
Brazilian Journal of Pharmaceutical Sciences, Vol 50, Iss 4, Pp 895-901 (2014)

Desenvolveu-se método específico, preciso, exato, linear, rápido e econômico, de validação de estabilidade, indicando o método de CLAE-FR para a quantificação simultânea de cefepima e tazobactam na forma de dosagem injetável seca. A separa

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::f379cc11002d837d931dcb5de3e08344
https://doi.org/10.1590/s1984-82502014000400025

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Validation of high performance liquid chromatographic and spectrophotometric methods for the determination of the antiparkinson agent pramipexole dihydrochloride monohydrate in pharmaceutical products

Autor: Serpil Sevim, Nevin Erk

Publikováno v: Brazilian Journal of Pharmaceutical Sciences; Vol. 51 No. 4 (2015); 879-891
Brazilian Journal of Pharmaceutical Sciences; Vol. 51 Núm. 4 (2015); 879-891
Brazilian Journal of Pharmaceutical Sciences; v. 51 n. 4 (2015); 879-891
Brazilian Journal of Pharmaceutical Sciences
Universidade de São Paulo (USP)
instacron:USP
Brazilian Journal of Pharmaceutical Sciences, Vol 51, Iss 4, Pp 879-891 (2015)
Brazilian Journal of Pharmaceutical Sciences, Volume: 51, Issue: 4, Pages: 879-891, Published: DEC 2015

The antiparkinson agent pramipexole dihydrochloride monohydrate was quantified in pharmaceutical products by high performance liquid chromatography (HPLC) and derivative spectrophotometry. The first method was based on HPLC using tamsulosin HCl as an

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::e49ef614ed9c6ffaa1fb639bd03dfe44
https://www.revistas.usp.br/bjps/article/view/118641

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Prevalence of hemoglobinopathies in school children: the importance of using confirmatory methods

Autor: Jacqueline da Silva Guimarães, Ana Maria de Souza, Cristiane Fernandes de Freitas Tavares

Publikováno v: Brazilian Journal of Pharmaceutical Sciences; Vol. 51 No. 2 (2015); 361-366
Brazilian Journal of Pharmaceutical Sciences; Vol. 51 Núm. 2 (2015); 361-366
Brazilian Journal of Pharmaceutical Sciences; v. 51 n. 2 (2015); 361-366
Brazilian Journal of Pharmaceutical Sciences
Universidade de São Paulo (USP)
instacron:USP
Brazilian Journal of Pharmaceutical Sciences, Vol 51, Iss 2, Pp 361-366 (2015)
Brazilian Journal of Pharmaceutical Sciences, Volume: 51, Issue: 2, Pages: 361-366, Published: JUN 2015

The hemoglobinopathies are included among the most common genetic diseases in the world. In Brazil, hemoglobinopathies are related to the diversity of racial backgrounds and the degree of interbreeding. The study focused on the prevalence of hemoglob

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::c3bf8952b0fbdc1fb63e2af4348a14da
https://www.revistas.usp.br/bjps/article/view/102407

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