Zobrazeno 1 - 10
of 69
pro vyhledávání: '"Harald Jancke"'
Publikováno v:
Rapid Communications in Mass Spectrometry. 17:285-290
Liquid chromatography in combination with spectroscopic methods like matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOFMS) or nuclear magnetic resonance (NMR) spectroscopy is a powerful method to characterize sils
Publikováno v:
BUNSEKI KAGAKU. 52:1029-1036
定量核磁気共鳴(NMR)法は測定原理から国際単位系に結び付く測定法として注目されているが,この方法を利用し高精度な定量測定を行った報告は少ない.定量NMR法を利用して,国際度
Publikováno v:
Zeitschrift für anorganische und allgemeine Chemie. 628:707-710
Raman spectroscopic and 35Cl-NMR scans of Hydro-Xan®, a preparation containing the biocatalytically effective Tetrachlorinedecaoxide anion (TCDO), are described. The spectroscopic analyses showed that HydroXan® does not contain chlorite initially u
Publikováno v:
Journal of Environmental Monitoring. 4:313-317
In 13C cross-polarisation magic angle spinning (CPMAS) spectra of soil samples, the paramagnetic soil constituents partially discriminate against the signal intensity of the 13C atoms. The aim of the present study was to check to what extent this sig
Autor:
Antonia Neels, Harald Jancke, Philip Pattison, Burhkard Costisella, Helen Stoeckli-Evans, Kenneth D. Knudsen
Publikováno v:
Helvetica Chimica Acta. 82:35-43
The structure of [(dimethylamino)methylene]bis[phosphonic acid] dihydrate (C3H11NO6P2⋅2 H2O; 1) was solved ab initio from synchrotron powder X-ray diffraction data. The structure determination was based on direct methods combined with difference Fo
Publikováno v:
Umweltwissenschaften und Schadstoff-Forschung. 11:9-14
Es werden vergleichende Untersuchungen zur Messung und Quantifizierung von Mineralolkohlenwasserstoffen (MKW) mittels Fourier-Transform-Infrarot (FT/IR)-Spektroskopie,1H-Kern-resonanz (1H-NMR)-Spektroskopie und Kapillargaschromato-graphie-Flammenioni
Publikováno v:
Solid State Nuclear Magnetic Resonance. 9:177-189
For alpha-quartz, monoclinic ZSM-5, alpha- and beta-Si3N4 and SiC-6H polytype, the silicon chemical shifts have been calculated using the IGLO (individual gauge for localized orbitals) method and models of different size in real crystal geometry. The
Publikováno v:
Main Group Chemistry. 2:17-30
The 29Si NMR chemical shifts of the methyl chlorine silanes (CH3)3-n Cl n SiX (n = 0…3) with X = H, CH3, C2H5, CH2Cl, CHCl2, NH2, N(H)CH3, N(CH3)2, OH, OCH3, OCH3, OC2H5, OSiH3, F, SiH3, and Cl have been calculated using the IGLO (Individual Gauge
Autor:
Gerald Zehl, Michael Bartoszek, Harald Jancke, Hiroyuki Isutzu, Kazuyuki Maeda, Fujio Mizukami, Luecke Bernhard, Stefan Bischoff
Publikováno v:
J. Mater. Chem.. 5:1893-1897
An improved method for the preparation of porous silica xerogels is described. Tetraethoxysilane (TEOS) as the starting alkoxide is modified by transesterification with 2-methylpentane-2,4-diol (MPD) prior to hydrolysis. The specific surface area and
Publikováno v:
Journal of Sol-Gel Science and Technology. 2:51-56
The reactivity of tetraethoxysilane (TEOS) used in many sol-gel syntheses can be increased by prehydrolysis. In contrast to one-step prehydrolysis acidic two-step prehydrolysis causes an increase of the reactivity of the low molecular species provide