Zobrazeno 1 - 10
of 33
pro vyhledávání: '"Hanna Małuszyńska"'
Publikováno v:
Symmetry, Vol 15, Iss 6, p 1172 (2023)
1,4- and 1,2-additons of secondary phosphine oxides to (1R)-myrtenal and (1S)-myrtanal were evaluated as potential routes to P,C-stereogenic phosphine oxides bearing additional hydroxyl or aldehyde functions. 1,4-Additions of racemic secondary phosph
Externí odkaz:
https://doaj.org/article/1699175308fc42fdbb1d89426be670d4
Autor:
Elżbieta Łastawiecka, Adam Włodarczyk, Anna E. Kozioł, Hanna Małuszyńska, K. Michał Pietrusiewicz
Publikováno v:
Molecules, Vol 26, Iss 22, p 6873 (2021)
The resolution of racemic 1-phenylphosphin-2-en-4-one 1-oxide (2), was achieved through the fractional crystallization of its diastereomeric complexes with (4R,5R)-(−)-2,2-dimethyl -α,α,α′,α′-tetraphenyl-dioxolan-4,5-dimethanol (R,R-TADDOL)
Externí odkaz:
https://doaj.org/article/eb5dc90824cf4b1387c8507a7284a917
Autor:
K. Michał Pietrusiewicz, Anna E. Koziol, Hanna Małuszyńska, Elżbieta Łastawiecka, Adam Włodarczyk
Publikováno v:
Molecules
Volume 26
Issue 22
Molecules, Vol 26, Iss 6873, p 6873 (2021)
Volume 26
Issue 22
Molecules, Vol 26, Iss 6873, p 6873 (2021)
The resolution of racemic 1-phenylphosphin-2-en-4-one 1-oxide (2), was achieved through the fractional crystallization of its diastereomeric complexes with (4R,5R)-(−)-2,2-dimethyl -α,α,α′,α′-tetraphenyl-dioxolan-4,5-dimethanol (R,R-TADDOL)
Autor:
Hanna Małuszyńska, Marek Stankevič, K. Michał Pietrusiewicz, Sylwia Sowa, Anna Szmigielska, Anna E. Koziol
Publikováno v:
The Journal of Organic Chemistry. 80:1672-1688
A direct stereoselective conversion of tertiary hydroxyalkylphosphine oxides to the corresponding tertiary hydroxyalkylphosphine-boranes involving facile reduction of the P═O bond by BH3 under mild conditions has been developed. The unprecedented f
Autor:
Maria Gdaniec, Hanna Małuszyńska
Publikováno v:
Journal of Molecular Structure. 983:141-146
A redetermination of the crystal structure of bis(thiourea) thiazolium bromide (hereafter T2ThBr) at 250 K (HT) and 100 K (LT) points to different space group symmetries than the ones reported in [A. Pajzderska, J. Wąsicki, H. Maluszynska, P. Czarne
Autor:
K. Michał Pietrusiewicz, Sylwia Sowa, Marek Stankevič, Anna Szmigielska, Anna E. Koziol, Hanna Małuszyńska
Publikováno v:
ChemInform. 46
The conversion of a variety of tertiary hydroxyalkylphosphine oxides to the corresponding phosphine boranes using BH3·THF or BH3·SMe2 as reagent is developed.
Publikováno v:
Journal of Physics: Condensed Matter. 15:5663-5674
The crystal and molecular structure of pyridinium periodate [H5C5NH]+[IO 4]− (hereafter referred to as PyIO4) was re-determined by single-crystal neutron diffraction at 350, 300 and 100 K. The structures of the high-temperature paraelectric and the
Publikováno v:
Zeitschrift für Naturforschung A. 57:847-853
By X-ray diffraction it was found that at 293 K the crystals of rubidium tetraphenylborate are tetragonal, space group I42m, a = b = 11.212(2) Å, c = 8.098(2) Å , with 2 molecules of Rb+[C24H20B]- in the unit cell. The molecular reorientations as f
Publikováno v:
The Journal of Chemical Physics. 117:5303-5310
The crystal and molecular structure of pyridinium fluorochromate has been determined at 293, 240, and 150 K by x-ray diffraction. All three phases are orthorhombic with the following sequence of space groups and solid–solid phase transitions disclo
Publikováno v:
Phase Transitions. 75:379-388
This paper illustrates the application of CW-EPR combined with the Computer Resolution Enhancement Method (CREM) to the investigation of the phase transitions and molecular dynamics of radicals in pyridinium perchlorate single crystals. The CREM meth