Zobrazeno 1 - 10
of 11
pro vyhledávání: '"György Bánsághi"'
Publikováno v:
Chemical Engineering & Technology. 41:1466-1472
Autor:
Sandra de Simón Brezmes, Edit Székely, György Bánsághi, János Madarász, Máté Zsemberi, Imre Miklós Szilágyi, László Lőrincz, Tamás Sohajda
Publikováno v:
The Journal of Supercritical Fluids. 118:48-53
We investigated the resolution and crystallization of ibuprofen with ( R )-phenylethylamine based on diastereomeric salt formation using the supercritical gas antisolvent (GAS) method. Our goal was to study the effects of the operational parameters (
Autor:
Erzsébet Varga, Tamás Sohajda, Edit Székely, György Bánsághi, Rita Bodáné Kendrovics, Zoltán Juvancz
Publikováno v:
Chromatographia. 78:881-888
Obtaining enantiomeric pure compounds is—among other techniques—possible in a resolvation experiment via diastereomeric salt formation, excellently exemplified by a modified Pope–Peachy method performed in supercritical carbon dioxide as solven
Autor:
Jorge Augustín Martínez Pérez, Dániel Varga, László Hegedűs, Béla Simándi, Edit Székely, Sandor Miskolczi, György Bánsághi
Publikováno v:
Chemical Engineering & Technology. 37:1885-1890
The chiral resolution of two racemic cyclopropanecarboxylic acids with the resolving agents (S)-2-(N-benzylamino)butan-1-ol and (R)-1-phenylethanamine was investigated. The resolutions were based on diastereomer salt crystallization in supercritical
Publikováno v:
Chemical Engineering & Technology. 37:1417-1421
The crystallization and resolution of cis-permethric acid (cPA) with (1R)-1-phenylethanamine (PhEA) as a resolving agent was investigated using the gas antisolvent (GAS) and supercritical antisolvent (SAS) methods. A significant pressure effect on bo
Publikováno v:
The Journal of Supercritical Fluids. 69:113-116
The first in situ diastereomeric salt formation reaction in supercritical carbon dioxide is reported in this paper. The reaction studied was the salt formation between racemic ibuprofen and ( R )-(1)-phenylethylamine, and was combined with supercriti
Autor:
Judit Halász, György Bánsághi, Dániel Varga, Béla Simándi, Edit Székely, György Pokol, János Madarász
Publikováno v:
Journal of Thermal Analysis and Calorimetry. 111:567-574
Two different compounds have formed from liquid enantiomeric (R-) and racemic α-methylbenzylamine (α-MBA, named also as 1-phenylethylamine, 1-FEA) with supercritical fluid CO2. The crystalline solids have been characterized by elemental CHN analysi
Autor:
László Vida, György Bánsághi, Péter Molnár, János Madarász, Béla Simándi, Edit Székely, Paul Thorey
Publikováno v:
Industrial & Engineering Chemistry Research. 49:9349-9354
A racemic mixture of trans-1,2-cyclohexanediol (CHD) is reacted with S,S- or R,R-tartaric acid in ethanol with a 0.5 or higher molar ratio of resolving agent to racemic CHD. The tartaric acid (TA) ...
Autor:
Péter Molnár, János Madarász, Petra Bombicz, László Párkányi, György Bánsághi, Imre Miklós Szilágyi, György Pokol, Béla Simándi, Edit Székely, Paul Thorey
Publikováno v:
Thermochimica Acta. 497:129-136
A novel co-crystal of trans-(R,R)-1,2-cyclohexanediol and (R,R)-tartaric acid (with 1:1 molar ratio, 1) has been found to be a key crystalline compound in the improved resolution of (±)-trans-1,2-cyclohexanediol by supercritical fluid extraction. Th
Autor:
György Bánsághi, László Poppe, Paul Thorey, Elemér Fogassy, Péter Molnár, Anna Tomin, Sándor Kemény, Béla Simándi, Edit Székely
Publikováno v:
Tetrahedron: Asymmetry. 19:1587-1592
A simple method for the resolution of racemic trans -1,2-cyclohexanediol enantiomers is presented in this paper. The chiral discrimination was performed by tartaric acid via diastereomeric complex formation. The diastereomeric complexes were formed b