Zobrazeno 1 - 10
of 13
pro vyhledávání: '"Grigory M. Lipkind"'
Publikováno v:
Canadian Journal of Chemistry. 68:1238-1250
1H and 13C NMR spectra have been recorded and the nuclear Overhauser enhancements (in D2O), after pre-irradiation of the anomeric protons, have been measured for tri- and tetrasaccharides containing 2,3-disubstituted residues of α-L-rhamnose and the
Publikováno v:
Carbohydrate research. 237
The syntheses are described of 2,3-di-O-glycosyl derivatives of methyl α- l - rhamnopyranoside (1–5)and α- d -mannopyranoside (6–9). Download : Download full-size image X Y X Y 1 α- l -Rha p α- d -Glc p 6 α- l -Rha p α- d -Glc p 2 α- d -Gl
Publikováno v:
Carbohydrate research. 223
The syntheses are described of 2,3-di-O-glycosyl derivatives (1-12) of methyl alpha-L-rhamnopyranoside where the glycosyl moieties are variously alpha-L-fucopyranose, beta-L-fucopyranose, beta-D-glucopyranose, alpha-D-mannopyranose, and alpha-L-rhamn
Publikováno v:
Carbohydrate research. 221
Conformational studies of the branched trisaccharide glycosides X-(1----2)[Y-(1----3)]-alpha-L-Rha-OMe (where X and Y are residues of alpha-L-, beta-L-, alpha-D-, and beta-D-hexopyranoses) were based on 1H- and 13C-n.m.r. data (n.O.e.'s, 13C chemical
Autor:
Nikolay K. Kochetkov, Elzbieta Romanowska, Nina A. Kocharova, Ewa Katzenellenbogen, Grigory M. Lipkind, Alexander S. Shashkov, Yuriy A. Knirel
Publikováno v:
Carbohydrate research. 203(2)
On mild acid-catalysed degradation of the lipopolysaccharide from Hafnia alvei O39 followed by gel filtration of Sephadex G-50, the O-specific polysaccharide and three oligosaccharides were obtained, which represent the core substituted with 0-2 O-an
Autor:
N. E. Nifant'ey, Grigory M. Lipkind, Barbara Jann, Alexander S. Shashkov, N. K. Kochetkov, Klaus Jann
Publikováno v:
Glycoconjugate Journal. 10:335-335
Publikováno v:
Carbohydrate Research. 133:1-13
A theoretical conformational analysis of the methyl β-glycosides of cellobiose and maltose was carried out and average values of the coupling constants 3 J C-1,H-4′ and 3 J C-4′,H-1 and optical linkage rotation (Λ) were calculated. It was shown
Publikováno v:
Carbohydrate Research. 181:1-12
Conformations of (1→2)-, (1→3)-, and (1→4)-linked disaccharide methyl glycosides involving aldohexopyranose residues have been studied on the basis of the inter-unit n.O.e. and theoretical calculations using atom-atom potential functions. The p
Publikováno v:
Carbohydrate Research. 147:175-182
A nuclear Overhauser enhancement in methyl β-maltoside, resulting from pre-irradiation of H-1′ of the non-reducing glucose residue, has been measured and calculated theoretically. Comparison of these data reveals a complicated conformational equil
Autor:
Alexander S. Shashkov, Nikolay K. Kochetkov, Yuriy A. Knirel, Grigory M. Lipkind, Evgeny V. Vinogradov
Publikováno v:
Carbohydrate Research. 175:59-75
A computerised approach to the structural analysis of unbranched regular polysaccharides is described, which is based on an evaluation of the 13C-n.m.r. spectra for all possible primary structures within the additive scheme starting from the chemical