Zobrazeno 1 - 10
of 66
pro vyhledávání: '"Gilles Févotte"'
Publikováno v:
IFAC Proceedings Volumes. 44:14025-14030
This paper deals with the control problem of crystallization processes. The dynamics of the system are governed by nonlinear partial differential equations, and the growth kinetics under consideration depends both on crystal size and on time. Given a
Publikováno v:
IFAC Proceedings Volumes. 44:10460-10465
Up to now, there is no sensor which permits to obtain an on-line measurement of the crystal size distribution in a batch crystallizer. Based on the measure of the concentration of the solute, this papers deals with the design of an observer which all
Autor:
François Févotte, Gilles Févotte
Publikováno v:
Scopus-Elsevier
Abstract For obvious industrial and theoretical reasons the problem of accounting for the effect of impurities in the population balance modelling of solution crystallization processes is a very important issue, and yet it has never been reported unt
Publikováno v:
Analytical Chemistry
Analytical Chemistry, American Chemical Society, 2008, 80 (17), pp.6658-6665. ⟨10.1021/ac800987m⟩
Analytical Chemistry, American Chemical Society, 2008, 80 (17), pp.6658-6665. ⟨10.1021/ac800987m⟩
International audience; There is an increasing interest in using Raman spectroscopy to identify polymorphic forms and monitor phase changes in pharmaceutical products for quality control. Compared with other analytical techniques for the identificati
Publikováno v:
Macromolecules
Macromolecules, American Chemical Society, 2008, 41 (14), pp.5166-5173. ⟨10.1021/ma800326x⟩
Macromolecules, American Chemical Society, 2008, 41 (14), pp.5166-5173. ⟨10.1021/ma800326x⟩
International audience; The kinetics of the miniemulsion copolymerization of styrene (St) and gamma-methacryloxypropyltrimethoxysilane (MPS) was investigated by studying the effects of the MPS/St weight ratio, the nature and amount of initiator, the
Publikováno v:
Chemical Engineering and Processing: Process Intensification
Chemical Engineering and Processing: Process Intensification, Elsevier, 2008, 47 (3), pp.377-382. ⟨10.1016/j.cep.2007.01.004⟩
Chemical Engineering and Processing: Process Intensification, Elsevier, 2008, 47 (3), pp.377-382. ⟨10.1016/j.cep.2007.01.004⟩
International audience; Citric acid exhibits two solid (anhydrous/monohydrate) phases in water. Below 34 °C, the more stable form being the monohydrate. This organic compound was selected as a model product to evaluate the continuous monitoring of s
Publikováno v:
Crystal Growth & Design
Crystal Growth & Design, American Chemical Society, 2007, 7 (10), pp.2088-2095. ⟨10.1021/cg0606343⟩
Crystal Growth & Design, American Chemical Society, 2007, 7 (10), pp.2088-2095
Crystal Growth & Design, American Chemical Society, 2007, 7 (10), pp.2088-2095. ⟨10.1021/cg0606343⟩
Crystal Growth & Design, American Chemical Society, 2007, 7 (10), pp.2088-2095
International audience; Experimental data about both the liquid and the solid phases during seeded batch crystallizations of citric acid (CA) in water were obtained using in situ Raman spectroscopy and image acquisition. These experimental results we
Autor:
Gilles Févotte
Publikováno v:
Chemical Engineering Research and Design. 85:906-920
As Raman spectroscopy enables complex, in situ, non-destructive and fast quantitative measurements of the solid state of pharmaceutical compounds, this technique is expected to allow the development of innovative future industrial applications for mo
Publikováno v:
IFAC Proceedings Volumes. 39:667-672
This paper deals with the problem of estimating CSD (Crystal Size Distributions) during polymorphic crystallization processes. The proposed approach is based on the high gain observer using the discretization of the PBE's (Population Balance Equation
Publikováno v:
International Journal of Pharmaceutics
International Journal of Pharmaceutics, Elsevier, 2006, 307 (2), pp.201-208. ⟨10.1016/j.ijpharm.2005.10.009⟩
International Journal of Pharmaceutics, Elsevier, 2006, 307 (2), pp.201-208. ⟨10.1016/j.ijpharm.2005.10.009⟩
International audience; A calibration strategy for the continuous monitoring of solvent-mediated phase transition was developed using in situ Raman spectroscopy. Citric acid which exhibits enantiotropy during its anhydrous/monohydrate phase transitio