Isolation of Caribbean Ciguatoxin-5 (C-CTX5) and confirmation of its structure by NMR spectroscopy.

Autor: Miles CO; Biotoxin Metrology, National Research Council, 1411 Oxford Street, Halifax, NS, B3H 3Z1 Canada.; Norwegian Veterinary Institute, P.O. Box 64, 1431 Ås, Norway., Burton IW; Aquatic and Crop Resources Development Research Center, National Research Council, 1411 Oxford Street, Halifax, NS, B3H 3Z1 Canada., Lewis NI; Biotoxin Metrology, National Research Council, 1411 Oxford Street, Halifax, NS, B3H 3Z1 Canada., Robertson A; Stokes School of Marine & Environmental Sciences, University of South Alabama, 600 Clinic Drive, Mobile, AL 36688, USA.; Marine Ecotoxicology Group, Dauphin Island Sea Lab, 101 Bienville Blvd, Dauphin Island, Dauphin Island, AL 36528, USA., Giddings SD; Biotoxin Metrology, National Research Council, 1411 Oxford Street, Halifax, NS, B3H 3Z1 Canada., McCarron P; Biotoxin Metrology, National Research Council, 1411 Oxford Street, Halifax, NS, B3H 3Z1 Canada., Mudge EM; Biotoxin Metrology, National Research Council, 1411 Oxford Street, Halifax, NS, B3H 3Z1 Canada.

Publikováno v: Tetrahedron [Tetrahedron] 2024 Aug 03; Vol. 162. Date of Electronic Publication: 2024 Jun 18.

Selective Extraction and Purification of Azaspiracids from Blue Mussels ( Mytilus edulis) Using Boric Acid Gel.

Autor: Miles CO; Norwegian Veterinary Institute, P.O. Box 750 Sentrum , N-0106 Oslo , Norway.; Measurement Science and Standards , National Research Council , 1411 Oxford Street , Halifax , Nova Scotia B3H 3Z1 , Canada., Kilcoyne J; Marine Institute, Rinville, Oranmore, Co., Galway H91 R673 , Ireland., McCarron P; Measurement Science and Standards , National Research Council , 1411 Oxford Street , Halifax , Nova Scotia B3H 3Z1 , Canada., Giddings SD; Measurement Science and Standards , National Research Council , 1411 Oxford Street , Halifax , Nova Scotia B3H 3Z1 , Canada., Waaler T; Norwegian Veterinary Institute, P.O. Box 750 Sentrum , N-0106 Oslo , Norway., Rundberget T; Norwegian Veterinary Institute, P.O. Box 750 Sentrum , N-0106 Oslo , Norway.; Norwegian Institute for Water Research , N-0349 Oslo , Norway., Samdal IA; Norwegian Veterinary Institute, P.O. Box 750 Sentrum , N-0106 Oslo , Norway., Løvberg KE; Norwegian Veterinary Institute, P.O. Box 750 Sentrum , N-0106 Oslo , Norway.

Publikováno v: Journal of agricultural and food chemistry [J Agric Food Chem] 2018 Mar 21; Vol. 66 (11), pp. 2962-2969. Date of Electronic Publication: 2018 Mar 12.

Development of Certified Reference Materials for Diarrhetic Shellfish Poisoning Toxins, Part 1: Calibration Solutions.

Autor: Beach DG; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1., Crain S; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1., Lewis N; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1., LeBlanc P; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1., Hardstaff WR; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1., Perez RA; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1., Giddings SD; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1., Martinez-Farina CF; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1., Stefanova R; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1., Burton IW; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1., Kilcoyne J; Marine Institute, Rinville, Oranmore, Galway County H91 R673, Ireland., Melanson JE; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1., Quilliam MA; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1., McCarron P; National Research Council Canada, Measurement Science and Standards, 1411 Oxford St, Halifax, NS, Canada B3H 3Z1.

Publikováno v: Journal of AOAC International [J AOAC Int] 2016 Sep; Vol. 99 (5), pp. 1151-62. Date of Electronic Publication: 2016 Aug 13.

Structure Elucidation, Relative LC-MS Response and In Vitro Toxicity of Azaspiracids 7-10 Isolated from Mussels (Mytilus edulis).

Autor: Kilcoyne J; †Marine Institute, Rinville, Oranmore, County Galway, Ireland.; ‡School of Chemical and Pharmaceutical Sciences, Dublin Institute of Technology, Kevin Street, Dublin 8, Ireland., Twiner MJ; §School of Medicine, Wayne State University, Detroit, Michigan 48202, United States., McCarron P; ⊥Measurement Science and Standards, Biotoxin Metrology, National Research Council Canada, 1411 Oxford Street, Halifax, Nova Scotia B3H 3Z1, Canada., Crain S; ⊥Measurement Science and Standards, Biotoxin Metrology, National Research Council Canada, 1411 Oxford Street, Halifax, Nova Scotia B3H 3Z1, Canada., Giddings SD; ⊥Measurement Science and Standards, Biotoxin Metrology, National Research Council Canada, 1411 Oxford Street, Halifax, Nova Scotia B3H 3Z1, Canada., Foley B; ‡School of Chemical and Pharmaceutical Sciences, Dublin Institute of Technology, Kevin Street, Dublin 8, Ireland., Rise F; ∥Department of Chemistry, University of Oslo, N-0315 Oslo, Norway., Hess P; ▽Ifremer, Laboratoire Phycotoxines, Rue de l'Ile d'Yeu, 44311 Nantes, France., Wilkins AL; ○Norwegian Veterinary Institute, P.O. Box 750 Sentrum, 0106 Oslo Norway., Miles CO; ○Norwegian Veterinary Institute, P.O. Box 750 Sentrum, 0106 Oslo Norway.; #Department of Pharmaceutical Chemistry, School of Pharmacy, University of Oslo, P.O. Box 1068 Blindern, N-0316 Oslo Norway.

Publikováno v: Journal of agricultural and food chemistry [J Agric Food Chem] 2015 May 27; Vol. 63 (20), pp. 5083-91. Date of Electronic Publication: 2015 May 12.

Analysis of β-N-methylamino-L-alanine (BMAA) in spirulina-containing supplements by liquid chromatography-tandem mass spectrometry.

Autor: McCarron P; National Research Council Canada, Measurement Science and Standards, Biotoxin Metrology, 1411 Oxford St, Halifax, NS B3H 3Z1, Canada., Logan AC; CAMNR, 23679 Calabasas Road Suite 542, Calabasas, CA 91302, USA., Giddings SD; National Research Council Canada, Measurement Science and Standards, Biotoxin Metrology, 1411 Oxford St, Halifax, NS B3H 3Z1, Canada., Quilliam MA; National Research Council Canada, Measurement Science and Standards, Biotoxin Metrology, 1411 Oxford St, Halifax, NS B3H 3Z1, Canada.

Publikováno v: Aquatic biosystems [Aquat Biosyst] 2014 Aug 08; Vol. 10, pp. 5. Date of Electronic Publication: 2014 Aug 08 (Print Publication: 2014).