Zobrazeno 1 - 10
of 40
pro vyhledávání: '"Frauke Schödel"'
Publikováno v:
IUCrData, Vol 5, Iss 6, p x200863 (2020)
In the title hemisolvate, C27H36BI3N2.0.5C6H6, the dihedral angles between the central heterocyclic ring and pendant benzene rings are 82.9 (8) and 88.7 (9)° and the complete benzene solvent molecule of crystallization is generated by a crystallogra
Externí odkaz:
https://doaj.org/article/6e5ef14ddd3f45c0a07f13a8fb551942
Publikováno v:
IUCrData, Vol 4, Iss 7, p x190959 (2019)
The molecular structure of the title compound, C18H15ISi, which crystallizes in the space group C2/c, does not exhibit any unusual features. Two weak C—H...π interactions may help to consolidate the packing. The present structure is not isostructu
Externí odkaz:
https://doaj.org/article/557700a61ffe4058b662005a09534961
Publikováno v:
Zeitschrift für anorganische und allgemeine Chemie. 646:264-267
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::990b149904f264e07fbea3d2eea80fd7
https://doi.org/10.1002/zaac.201900304
https://doi.org/10.1002/zaac.201900304
Publikováno v:
IUCrData. 5(Pt 6)
In the title hemisolvate, C
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=pmid________::c31aba29c4d0fd19fc0021440a5d1114
https://pubmed.ncbi.nlm.nih.gov/36340616
https://pubmed.ncbi.nlm.nih.gov/36340616
Autor:
Jens Michael Breunig, Michael Bolte, Hans-Wolfram Lerner, Vasco Thiel, Frauke Schödel, Matthias Wagner
Publikováno v:
Zeitschrift für Naturforschung B. 72:747-752
The diazaborole Me3Sn–B{N(Dipp)CH}2 (1; B{N(Dipp)CH}2=N,N′-bis(2,6-diisopropylphenyl)-2,3-dihydro-1H-1,3,2-diazaborolyl) was prepared by the reaction of Me3SnCl with one equivalent of Li[B{N(Dipp)CH}2]. Single crystals of 1 were obtained from hex
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::976e5f9eb32061395947b1e2612416bf
https://doi.org/10.1515/znb-2017-0122
https://doi.org/10.1515/znb-2017-0122
Publikováno v:
Zeitschrift für Naturforschung B. 71:135-139
Treatment of P4with one equivalent of Li[SitBu3] leads to the formation of a number of oligo-phosphanes and -phosphides, e.g. the bicyclo[1.1.0]tetraphosphane P4(SitBu3)2, the heptaphosphanortricyclane P7(SitBu3)3, the tetraphosphides Li3[P(PSitBu3)3
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::7f07b7356df9ab0310e4a924b2733016
https://doi.org/10.1515/znb-2015-0156
https://doi.org/10.1515/znb-2015-0156
Unexpected Silaazetidine Formation in the Thermolysis of thf-Supported Silanimine Et2Si=N-SitBu3·thf
Publikováno v:
Zeitschrift für anorganische und allgemeine Chemie. 642:96-100
The silyl amide Et2SiCl-NLi-SitBu3 can be cleanly prepared from precursor silylamine Et2SiCl-NH-SitBu3 and Li[nBu]. The CF3SO3SiMe3 induced LiCl elimination of Et2SiCl-NLi-SitBu3 in thf afforded a 2-silaazetidine derivative by [2+2] cycloaddition of
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::ddbf0feb155388e9e07a30572a8cb976
https://doi.org/10.1002/zaac.201500691
https://doi.org/10.1002/zaac.201500691
Publikováno v:
Zeitschrift für Naturforschung B. 70:111-114
The thf-complexed silanimine tBu2Si=N–Sit- Bu3·thf (1(thf); monoclinic, space group C2/c) was prepared by the reaction of 1 equivalent of tBu2SiClN3 with 1 equivalent of Na[SitBu3] in Bu2O and subsequent addition of thf. By heating a benzene solut
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::e7111e356d3ce60f3aff16d52b195e65
https://doi.org/10.1515/znb-2014-0220
https://doi.org/10.1515/znb-2014-0220
Autor:
Inge Sänger, Günter Margraf, Hans-Wolfram Lerner, Matthias Wagner, Michael Bolte, Frauke Schödel
Publikováno v:
Zeitschrift für Naturforschung B. 67:549-556
The bis(trimethyl)silylamido complex Na(THF){Fe[N(SiMe3)2]3} and the disilane tBu3SiSitBu3 were obtained from the reaction of Fe[N(SiMe3)2]3 with the sodium silanide Na(THF)2[SitBu3] in a mixture of benzene and THF. Single crystals of Na(THF){Fe[N(Si
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::4868a5b35667dcc210adabbcdc7c2d60
https://doi.org/10.5560/znb.2012-0060
https://doi.org/10.5560/znb.2012-0060
Publikováno v:
Zeitschrift für Naturforschung B. 66:695-699
Single crystals suitable for X-ray diffraction of (tBu2P)3Ga (monoclinic, space group Cc) were obtained from GaCl3 and two equivalents of Li[PtBu2] at room temperature in benzene. The phosphanylgallane (tBu2P)3Ga was also produced via a one-pot appro
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::a466f7ded9ee08f7ff30d90859e030d7
https://doi.org/10.1515/znb-2011-0708
https://doi.org/10.1515/znb-2011-0708