Zobrazeno 1 - 10
of 41
pro vyhledávání: '"Fabio Simonelli"'
Autor:
Caroline Werner Pereira da Silva Grandizoli, Francinete Ramos Campos, Fabio Simonelli, Andersson Barison
Publikováno v:
Química Nova, Vol 37, Iss 7, Pp 1227-1232 (2014)
This work shows the application of ¹H NMR spectroscopy and chemometrics for quality control of grape juice. A wide range of quality assurance parameters were assessed by single ¹H NMR experiments acquired directly from juice. The investigation reve
Externí odkaz:
https://doaj.org/article/130269e6ca3142cd93e2cf72bab2ee8e
Autor:
Murilo B. M. de Mello, Alfredo R. M. de Oliveira, Fabio Simonelli, Maria de Fátima Costa Santos, Anderson Barison, Leandro Piovan
Publikováno v:
Journal of Organometallic Chemistry. 806:54-59
Alkylation or arylation of selenide or diselenide anions is a well-established method to obtain organoselenium compounds. Nevertheless, detecting inorganic selenium anions using 77Se NMR is still a challenge. In a previous work, alkylation of Na2Se w
Autor:
Noemi Nagata, Andersson Barison, João Luiz T. Ribas, Cinthia R. Souza, Aline Hara da Silva, Fabio Simonelli
Publikováno v:
Energy & Fuels. 28:4958-4962
The cetane number (CN) is one of the most important parameters regarding diesel fuel oil quality, mainly ignition properties. Traditionally, the CN determination is performed by a quite laborious and high-cost method on an explosion engine. On the ot
Autor:
Fabio Simonelli, Rogério A. Gariani, Jaísa F. Soares, Peter B. Hitchcock, Franciele de Oliveira, Giovana G. Nunes, Rúbia C. R. Bottini, Eduardo L. de Sá, Davi F. Back, Ernesto Schulz Lang, César de O. Cavalcanti, David J. Evans, Nevilde de L. G. da Rocha
Publikováno v:
European Journal of Inorganic Chemistry. 2010:2476-2487
The reaction of anhydrous FeCl 2 with 2-(4',4'-dimethylox-azolin-2'-yl)thiophenolate (ox-phS - ) afforded mononuclear [Fe(ox-phS) 2 ] (A) and binuclear [(Fe III (ox-phS)} 2 (μ-S) 2 ] (B). In B, iron(III) and S 2- resulted from an unexpected redox re
Autor:
Rogério A. Gariani, Fabio Simonelli, Alfredo R. M. de Oliveira, João V. Comasseto, Andersson Barison
Publikováno v:
Tetrahedron: Asymmetry. 17:2930-2934
The tellurium nuclear magnetic resonance spectrum of chiral tellurium ferrocene 2 produces a single signal at different chemical shifts when solubilized together with different enantiomeric proportions of chiral compounds.
Publikováno v:
Tetrahedron Letters. 46:2539-2542
A series of common organometallic reagents were used in the reaction with an acyclic and a cyclic activated 2-alkenyl aziridines and the selectivity aspects for each aziridine was addressed.
Autor:
Giuliano C. Clososki, Fabio Simonelli, Alfredo R. M. de Oliveira, Paulo H. G. Zarbin, Francisco A. de Marques, Alcindo A. Dos Santos
Publikováno v:
Synlett. :0975-0978
This paper describes the preparation of a series of oxazoline cuprates by reaction of an oxazoline lithium anion with copper(I) salts: CuBr.DMS, Cul and CuCN in THF solution. The oxazoline cyanocuprate showed the best reactivity using enones as elect
Autor:
Francinete Ramos Campos, Fabio Simonelli, Luise Z. B. Carrenho, Arquimedes Paixão de Santana Filho, Guilherme L. Sassaki, Caroline W. P. da S. Grandizoli, Maria Regina O. Kreuger, Noemi Nagata, Andersson Barison, Thais Martins Guimarães de Francisco
Publikováno v:
Journal of the Brazilian Chemical Society.
The success of cancer treatment is directly related to early detection before symptoms emerge, although nowadays few cancers can be detected early. In this sense, 1H nuclear magnetic resonance (1H NMR)-based metabonomics was used to identify metaboli
Publikováno v:
Química Nova.
This work shows the application of 1H NMR spectroscopy and chemometrics for quality control of grape juice. A wide range of quality assurance parameters were assessed by single 1H NMR experiments acquired directly from juice. The investigation reveal
Autor:
Alcindo A. Dos Santos, Paulo H. G. Zarbin, Giuliano C. Clososki, Francisco A. Marques, Fabio Simonelli, Alfredo R. M. de Oliveira
Publikováno v:
Tetrahedron Letters. 42:7375-7378
Current studies of oxazoline cyanocuprates addition to conjugated nitroalkenes, and their improved reactivity when compared to lithium oxazoline anions, has shown to be an efficient method for the synthesis of a variety of γ-nitrooxazolines, an inte