Synthesis and Structural Studies of peri-Substituted Acenaphthenes with Tertiary Phosphine and Stibine Groups

Autor: Laurence J. Taylor, Emma E. Lawson, David B. Cordes, Kasun S. Athukorala Arachchige, Alexandra M. Z. Slawin, Brian A. Chalmers, Petr Kilian

Publikováno v: Molecules, Vol 29, Iss 8, p 1841 (2024)

Two mixed peri-substituted phosphine-chlorostibines, Acenap(PiPr2)(SbPhCl) and Acenap(PiPr2)(SbCl2) (Acenap = acenaphthene-5,6-diyl) reacted cleanly with Grignard reagents or nBuLi to give the corresponding tertiary phosphine-stibines Acenap(PiPr2)(S

Externí odkaz: https://doaj.org/article/ae643bc614444578b38f53fc04c7bbc0

SIGNET: protocol for a multicentre, single-blind prospective, group sequential, randomised controlled trial to evaluate the benefits of a single dose of simvastatin given to potential organ donors declared dead by neurological criteria on outcomes in organ recipients.

Autor: Evans A; Clinical Trials Unit, NHS Blood and Transplant, Cambridge, UK., Mawson P; Newcastle University Faculty of Medical Sciences, Newcastle upon Tyne, UK Phil.Mawson@newcastle.ac.uk., Thomas H; Clinical Trials Unit, NHS Blood and Transplant, Bristol, UK., Keen K; Clinical Trials Unit, NHS Blood and Transplant, Cambridge, UK., Watson CJ; Department of Surgery, University of Cambridge and the NIHR Cambridge Biomedical Research Centre, Cambridge, UK., McAuley DF; Centre for Experimental Medicine, Queen's University Belfast, Belfast, UK., MacGowan GA; Newcastle University Faculty of Medical Sciences, Newcastle upon Tyne, UK.; Newcastle Upon Tyne Hospitals NHS Foundation Trust, Newcastle Upon Tyne, UK., Sheerin NS; Newcastle University Faculty of Medical Sciences, Newcastle upon Tyne, UK., Fisher A; Newcastle University Faculty of Medical Sciences, Newcastle upon Tyne, UK., Shaw J; Newcastle University Faculty of Medical Sciences, Newcastle upon Tyne, UK., Yates H; Patient and Public Involvement, Newcastle upon Tyne, UK., Fallow A; Patient and Public Involvement, Newcastle upon Tyne, UK., Kounali D; Clinical Trials Unit, NHS Blood and Transplant, Bristol, UK., Banks J; Clinical Trials Unit, NHS Blood and Transplant, Bristol, UK., Stevens M; NHS Blood and Transplant Organ Donation, Cambridge, UK., Paul R; Clinical Trials Unit, NHS Blood and Transplant, Cambridge, UK., Hodge R; Clinical Trials Unit, NHS Blood and Transplant, Cambridge, UK., Lawson E; NHS Blood and Transplant Organ Donation, Cambridge, UK., Harvey D; Adult Intensive Care, Nottingham University Hospitals NHS Trust, Nottingham, UK.; NHS Blood & Transplant Organ Donation, Bristol, UK., Dark J; Newcastle University Faculty of Medical Sciences, Newcastle upon Tyne, UK.

Publikováno v: BMJ open [BMJ Open] 2024 Sep 18; Vol. 14 (9), pp. e086352. Date of Electronic Publication: 2024 Sep 18.