Zobrazeno 1 - 10
of 11
pro vyhledávání: '"Edward R. Grover"'
Publikováno v:
Journal of Chromatography A. 792:385-391
The 1-phenyl-3-methyl-5-pyrazolone (PMP) derivatives of aldose enantiomers were well separated from each other by capillary zone electrophoresis using a neutral phosphate buffer containing an optically active N-dodecoxycarbonylvaline (DCV). The l -en
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::e11126f81f97a89d7754a6471fa35e4b
https://doi.org/10.1016/s0021-9673(97)00926-6
https://doi.org/10.1016/s0021-9673(97)00926-6
Publikováno v:
Journal of Chromatography A. 735:303-310
The first report on the feasibility of method validation for the separation of enantiomeric mixtures by chiral micelle electrokinetic capillary chromatography is described. Method validation data elements were investigated according to U.S. Pharmacop
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::de678c5dd2b45d2e7c5490736d0f909d
https://doi.org/10.1016/0021-9673(95)00746-6
https://doi.org/10.1016/0021-9673(95)00746-6
Autor:
Edward R. Grover, Michael E. Swartz, Hassan Y. Aboul-Enein, Jeffrey R. Mazzeo, Phyllis R. Brown
Publikováno v:
Journal of Chromatography A. 724:307-316
The enantioselective separation of five racemic piperidine-2,6-dione compounds was accomplished using chiral micelle electrokinetic capillary chromatography. This class of drugs includes glutethimide, aminoglutethimide, cyclohexylaminoglutethimide, p
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::386211738cfa0669843b1d6cf54c7e67
https://doi.org/10.1016/0021-9673(95)00919-1
https://doi.org/10.1016/0021-9673(95)00919-1
Publikováno v:
Analytical Biochemistry. 231:65-71
A synthetic chiral surfactant was employed for the enantioselective micellar electrokinetic capillary chromatographic (MECC) separation of amino acid enantiomers derivatized with 6-aminoquinoyI- N -hydroxysuccinimidyl carbamate (AQC). The effect of s
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::8d14199ab824229a93f9702307bff065
https://doi.org/10.1006/abio.1995.1504
https://doi.org/10.1006/abio.1995.1504
Publikováno v:
Analytical Chemistry. 67:2966-2973
A resolution equation for electrokinetic chromatography (EKC) was developed starting from the resolution equation for electrophoresis. The equation was used to predict the influences of the migration window and partitioning on resolution in EKC. It i
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::8ef359e97ca75f5679bd5db8ab7d84be
https://doi.org/10.1021/ac00113a035
https://doi.org/10.1021/ac00113a035
Publikováno v:
Journal of Chromatography A. 680:125-135
A novel chiral surfactant was prepared as both enantiomeric forms, (R)- and (S)-N-dodecoxycarbonylvaline, and employed for the separation of enantiomeric mixtures by micellar electrokinetic capillary chromatography (MECC). The enantioselectivities (a
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::4657c1e5fac01360b80fb7cc1291c523
https://doi.org/10.1016/0021-9673(94)80060-x
https://doi.org/10.1016/0021-9673(94)80060-x
Autor:
Edward R. Grover, W.Harry Mandeville, Andrea Weston, Bonnie Bell-Alden, Wayne Sawlivich, George Vella, Robert Allan Mastico, Dorothy J. Phillips, Mark Cava
Publikováno v:
Journal of Chromatography A. 536:95-106
The use of a rigid silica-based packing material with large particle and pore size, 37–55 μm and 500 A pore, for affinity chromatography makes it possible to combine high selectivity with short analysis times. Both large and small molecules have b
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::b8faad822285b92fdf6f77e623def142
https://doi.org/10.1016/s0021-9673(01)89239-6
https://doi.org/10.1016/s0021-9673(01)89239-6
Autor:
Eric S. Grumbach, Bonnie A. Alden, Pamela C. Iraneta, Uwe D. Neue, Edward R. Grover, Alberto Méndez
In this chapter on HPLC columns, we are discussing both the surface chemistry of a packing as well as column design and performance. In the section that covers column chemistry, we cover modern options of base materials as well as the commonly used a
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::5268ae117b89374949e9392d0f5c9fed
https://doi.org/10.1016/s0149-6395(07)80009-2
https://doi.org/10.1016/s0149-6395(07)80009-2
Publikováno v:
Handbook of Capillary Electrophoresis Applications ISBN: 9789401071970
The separation of enantiomers by the mode of capillary electrophoresis termed micelle electrokinetic chromatography is reviewed. Topics include indirect separations accomplished by derivatization with chiral reagents and direct separations using cycl
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::41d2fcb524edda34947188a2de897832
https://doi.org/10.1007/978-94-009-1561-9_27
https://doi.org/10.1007/978-94-009-1561-9_27
Publikováno v:
Journal of the American Chemical Society. 102:6365-6369
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::e2d9996a80209c48ea2f017030b3589b
https://doi.org/10.1021/ja00540a045
https://doi.org/10.1021/ja00540a045