Efficient preparation of 5,10,15,20-tetrakis(4-bromophenyl)porphyrin. Microwave assisted v/s conventional synthetic method, X-ray and hirshfeld surface structural analysis

Autor: Edison Matamala-Cea, Rodrigo Arancibia, Néstor Novoa, Jean-René Hamon, Déborah González, Vincent Dorcet, Fabián Valenzuela-Godoy

Publikováno v: Journal of Molecular Structure
Journal of Molecular Structure, Elsevier, 2020, 1201, pp.127139. ⟨10.1016/j.molstruc.2019.127139⟩
Journal of Molecular Structure, 2020, 1201, pp.127139. ⟨10.1016/j.molstruc.2019.127139⟩

International audience; The symmetrical meso-tetrasubstituted porphyrin 5,10,15,20-tetrakis(4-bromophenyl)Porphyrin (1) has been synthesized in quite high yields, ranging from 55 – 78%, by conventional and microwave assisted techniques, and isolate

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https://hal-univ-rennes1.archives-ouvertes.fr/hal-02367901/document