Zobrazeno 1 - 10
of 25
pro vyhledávání: '"E. Duemichen"'
Publikováno v:
Journal of Chromatography A. 1592:133-142
The TED-GC–MS analysis is a two-step method. A sample is first decomposed in a thermogravimetric analyzer (TGA) and the gaseous decomposition products are then trapped on a solid-phase adsorber. Subsequently, the solid-phase adsorber is analyzed wi
Publikováno v:
Thermochimica Acta. 650:8-17
Non-isothermal heating rate kinetics was applied to two epoxy resin systems. In situ near-infrared (NIR) measurements were taken with a heatable NIR cell which allowed the cure to be monitored by characteristic absorption bands. An autocatalyzed reac
Publikováno v:
Polymer Degradation and Stability. 174:109032
Thermoset materials characterization is often limited to solid state analytical techniques such as IR, NMR, DSC, TGA and mechanical testing. Alternatively, their off-gassing behavior can also be evaluated using GC based techniques such as TD-GC-MS, a
Publikováno v:
Thermochimica Acta. 623:72-79
In this work a novel iterative method for isothermal cure kinetic modelling of an epoxy resin system using differential scanning calorimetry (DSC) technique is presented. To reach the isothermal cure temperature, the sample has to be heated up from a
Publikováno v:
Polymer Degradation and Stability. 120:340-356
The thermal molecular degradation of polyamide 66 (PA 66) doped with (partially supported) metal oxide particles (Fe 2 O 3 , ZnO, Al 2 O 3 ) was investigated qualitatively and quantitatively using common analysis techniques like thermogravimetry coup
Autor:
Ulrike Braun, Gerhard Ziegmann, Heinz Sturm, E. Duemichen, Maren Erdmann, Volker Trappe, M. Javdanitehran
Publikováno v:
Thermochimica Acta. 616:49-60
Near-infrared spectroscopy (NIR) turned out to be well suited for analyzing the degree of cure for epoxy systems. In contrast to dynamic scanning calorimetry (DSC), where the released heat of reaction determines the degree of epoxy conversion indirec
Autor:
Roland Becker, Ulrike Braun, E. Duemichen, Heinz Sturm, Paul Eisentraut, Jana Falkenhagen, Anna Maria Elert
Publikováno v:
Environmental pollution (Barking, Essex : 1987). 231(Pt 2)
In recent years, an increasing trend towards investigating and monitoring the contamination of the environment by microplastics (MP) (plastic pieces < 5 mm) has been observed worldwide. Nonetheless, a reliable methodology that would facilitate and au
Publikováno v:
Journal of Chromatography A. 1354:117-128
For analysis of the gaseous thermal decomposition products of polymers, the common techniques are thermogravimetry, combined with Fourier transformed infrared spectroscopy (TGA-FTIR) and mass spectrometry (TGA-MS). These methods offer a simple approa
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