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pro vyhledávání: '"E J, Kentzer"'
Publikováno v:
Journal - Association of Official Analytical Chemists. 71(2)
Amprolium is extracted with methanol-water (2 + 1) containing 5mM dioctylsulfosuccinate (DOSS) and 10mM CaCl2. The analyte is separated from coextracted materials by isocratic ion-pair reverse-phase liquid chromatography, following removal of late-el
Autor:
R L, Smallidge, E J, Kentzer, K R, Stringham, E H, Kim, C, Lehe, R W, Stringham, E C, Mundell
Publikováno v:
Journal - Association of Official Analytical Chemists. 71(4)
Twenty g sample, to which sulfamerazine has been added as internal standard, is extracted with 0.3N HCl + 1.5% diethylamine in 25% methanol. The sample extract is chilled (to aid clarification), centrifuged, and filtered. The sulfonamides are separat