Crystal structures of (R S)-N-[(1R,2S)-2-benz­yloxy-1-(2,6-di­methyl­phen­yl)prop­yl]-2-methyl­propane-2-sulfinamide and (R S)-N-[(1S,2R)-2-benz­yloxy-1-(2,4,6-tri­methyl­phen­yl)prop­yl]-2-methyl­propane-2-sulfinamide: two related protected 1,2-amino alcohols

Autor: Carbone, Matthew R., Centola, Garrick A., Haas, Adam, McClelland, Kevin P., Moskowitz, Michael D., Verderame, Angelo M., Olezeski, Mikael S., Papa, Louis J., Dorn, Stephanie C. M., Brennessel, William W., Weix, Daniel J.

Publikováno v: Acta Crystallographica Section E: Structure Reports

Mol­ecules of two related 1,2-amino alcohols are linked via N—H⋯O=S hydrogen bonds, forming chains along [100] for the first compound and along [010] for the second compound.
The title compounds, C22H31NO2S, (1), and C23H33NO2S, (2), are re

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http://europepmc.org/articles/PMC4257314

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ChemInform Abstract: Nickel-Catalyzed Reductive Arylation of Activated Alkynes with Aryl Iodides.

Autor: Dorn, Stephanie C. M., Olsen, Andrew K., Kelemen, Rachel E., Shrestha, Ruja, Weix, Daniel J.

Publikováno v: ChemInform; Sep2015, Vol. 46 Issue 39, pno-no, 1p

Bis{(R)-N-[(R)-2-benz-yloxy-1-(4-tert-butyl-phen-yl)eth-yl]-2-methyl-propane-2-sulfinamide} monohydrate.

Autor: Humes CL; Department of Chemistry, 120 Trustee Road, 412 Hutchison Hall, University of Rochester, Rochester, NY 14627, USA., Banker TJ; Department of Chemistry, 120 Trustee Road, 412 Hutchison Hall, University of Rochester, Rochester, NY 14627, USA., Dorn SC; Department of Chemistry, 120 Trustee Road, 412 Hutchison Hall, University of Rochester, Rochester, NY 14627, USA., Shanahan JP; Department of Chemistry, 120 Trustee Road, 412 Hutchison Hall, University of Rochester, Rochester, NY 14627, USA., Brennessel WW; Department of Chemistry, 120 Trustee Road, 412 Hutchison Hall, University of Rochester, Rochester, NY 14627, USA., Weix DJ; Department of Chemistry, 120 Trustee Road, 412 Hutchison Hall, University of Rochester, Rochester, NY 14627, USA.

Publikováno v: Acta crystallographica. Section E, Structure reports online [Acta Crystallogr Sect E Struct Rep Online] 2014 Mar 08; Vol. 70 (Pt 4), pp. o405-6. Date of Electronic Publication: 2014 Mar 08 (Print Publication: 2014).