NIST Interlaboratory Study on Glycosylation Analysis of Monoclonal Antibodies: Comparison of Results from Diverse Analytical Methods.

Autor: De Leoz MLA; Mass Spectrometry Data Center, Biomolecular Measurement Division, Material Measurement Laboratory, National Institute of Standards and Technology, 100 Bureau Drive Gaithersburg, Maryland 20899. Electronic address: lornadeleoz@gmail.com., Duewer DL; Chemical Sciences Division, Material Measurement Laboratory, National Institute of Standards and Technology, 100 Bureau Drive Gaithersburg, Maryland 20899., Fung A; Analytical Development, Agensys, Inc., 1800 Steward Street Santa Monica, California 90404., Liu L; Analytical Development, Agensys, Inc., 1800 Steward Street Santa Monica, California 90404., Yau HK; Analytical Development, Agensys, Inc., 1800 Steward Street Santa Monica, California 90404., Potter O; Agilent Technologies, Inc., 5301 Stevens Creek Blvd Santa Clara, California 95051., Staples GO; Agilent Technologies, Inc., 5301 Stevens Creek Blvd Santa Clara, California 95051., Furuki K; Astellas Pharma, 5-2-3 Tokodai, Tsukiba, Ibaraki, 300-2698, Japan., Frenkel R; Analytical Development, Biogen, 14 Cambridge Center Cambridge, Massachusetts 02142., Hu Y; Analytical Development, Biogen, 14 Cambridge Center Cambridge, Massachusetts 02142., Sosic Z; Analytical Development, Biogen, 14 Cambridge Center Cambridge, Massachusetts 02142., Zhang P; Bioprocessing Technology Institute, 20 Biopolis Way, Level 3 Singapore 138668., Altmann F; Department of Chemistry, University of Natural Resources and Life Science, Vienna (BOKU), Muthgasse 18 1190 Wien, Austria., Grunwald-Grube C; Department of Chemistry, University of Natural Resources and Life Science, Vienna (BOKU), Muthgasse 18 1190 Wien, Austria., Shao C; Center for Biomedical Mass Spectrometry, Boston University School of Medicine, 670 Albany Street Boston, Massachusetts 02118., Zaia J; Center for Biomedical Mass Spectrometry, Boston University School of Medicine, 670 Albany Street Boston, Massachusetts 02118., Evers W; Bruker Daltonik GmbH, Fahrenheitstr. 4, 28359 Bremen, Germany., Pengelley S; Bruker Daltonik GmbH, Fahrenheitstr. 4, 28359 Bremen, Germany., Suckau D; Bruker Daltonik GmbH, Fahrenheitstr. 4, 28359 Bremen, Germany., Wiechmann A; Bruker Daltonik GmbH, Fahrenheitstr. 4, 28359 Bremen, Germany., Resemann A; Bruker Daltonik GmbH, Fahrenheitstr. 4, 28359 Bremen, Germany., Jabs W; Bruker Daltonik GmbH, Fahrenheitstr. 4, 28359 Bremen, Germany; Department of Life Sciences & Technology, Beuth Hochschule für Technik Berlin, Seestraβe 64, 13347 Berlin, Germany., Beck A; Centre d'Immunologie Pierre Fabre, 5 Avenue Napoléon III, BP 60497, 74164 St Julien-en-Genevois, France., Froehlich JW; Department of Urology, Boston Children's Hospital, 300 Longwood Avenue Boston Massachusetts 02115., Huang C; Institute of Biophysics, Chinese Academy of Sciences, 15 Da Tun Road, Chaoyang District, Beijing 100101 China., Li Y; Institute of Biophysics, Chinese Academy of Sciences, 15 Da Tun Road, Chaoyang District, Beijing 100101 China., Liu Y; Institute of Biophysics, Chinese Academy of Sciences, 15 Da Tun Road, Chaoyang District, Beijing 100101 China., Sun S; Key Lab of Intelligent Information Processing, Institute of Computing Technology, Chinese Academy of Sciences, 15 Da Tun Road, Chaoyang District, Beijing 100101 China., Wang Y; Key Lab of Intelligent Information Processing, Institute of Computing Technology, Chinese Academy of Sciences, 15 Da Tun Road, Chaoyang District, Beijing 100101 China., Seo Y; Graduate School of Analytical Science and Technology, Chungnam National University, Gung-dong 220, Yuseong-Gu, Daejeon 305-764, Korea (South)., An HJ; Graduate School of Analytical Science and Technology, Chungnam National University, Gung-dong 220, Yuseong-Gu, Daejeon 305-764, Korea (South)., Reichardt NC; CICbiomaGUNE, Paseo Miramon 182, 20009 San Sebastian, Spain., Ruiz JE; CICbiomaGUNE, Paseo Miramon 182, 20009 San Sebastian, Spain., Archer-Hartmann S; Analytical Services, Complex Carbohydrate Research Center, University of Georgia, 315 Riverbend Road Athens, Georgia 30602., Azadi P; Analytical Services, Complex Carbohydrate Research Center, University of Georgia, 315 Riverbend Road Athens, Georgia 30602., Bell L; BioCMC Solutions (Large Molecules), Covance Laboratories Limited, Otley Road, Harrogate, North Yorks HG3 1PY, United Kingdom., Lakos Z; Biochemistry Method Development & Validation, Eurofins Lancaster Laboratories, Inc., 2425 New Holland Pike Lancaster, Pennsylvania 17601., An Y; Center for Biologics Evaluation and Research, Food and Drug Administration, 10903 New Hampshire Avenue, Silver Spring, Maryland 20993., Cipollo JF; Center for Biologics Evaluation and Research, Food and Drug Administration, 10903 New Hampshire Avenue, Silver Spring, Maryland 20993., Pucic-Bakovic M; Glycoscience Research Laboratory, Genos, Borongajska cesta 83h, 10 000 Zagreb, Croatia., Štambuk J; Glycoscience Research Laboratory, Genos, Borongajska cesta 83h, 10 000 Zagreb, Croatia., Lauc G; Glycoscience Research Laboratory, Genos, Borongajska cesta 83h, 10 000 Zagreb, Croatia; Faculty of Pharmacy and Biochemistry, University of Zagreb, A. Kovačića 1, 10 000 Zagreb, Croatia., Li X; Department of Chemistry, Georgia State University, 100 Piedmont Avenue, Atlanta, Georgia 30303., Wang PG; Department of Chemistry, Georgia State University, 100 Piedmont Avenue, Atlanta, Georgia 30303., Bock A; glyXera GmbH, Brenneckestrasse 20 * ZENIT / 39120 Magdeburg, Germany., Hennig R; glyXera GmbH, Brenneckestrasse 20 * ZENIT / 39120 Magdeburg, Germany., Rapp E; glyXera GmbH, Brenneckestrasse 20 * ZENIT / 39120 Magdeburg, Germany; AstraZeneca, Granta Park, Cambridgeshire, CB21 6GH United Kingdom., Creskey M; Health Products and Foods Branch, Health Canada, AL 2201E, 251 Sir Frederick Banting Driveway, Ottawa, Ontario, K1A 0K9 Canada., Cyr TD; Health Products and Foods Branch, Health Canada, AL 2201E, 251 Sir Frederick Banting Driveway, Ottawa, Ontario, K1A 0K9 Canada., Nakano M; Graduate School of Advanced Sciences of Matter, Hiroshima University, 1-3-1 Kagamiyama Higashi-Hiroshima 739-8530 Japan., Sugiyama T; Graduate School of Advanced Sciences of Matter, Hiroshima University, 1-3-1 Kagamiyama Higashi-Hiroshima 739-8530 Japan., Leung PA; ImmunoGen, 830 Winter Street, Waltham, Massachusetts 02451., Link-Lenczowski P; Department of Medical Physiology, Jagiellonian University Medical College, ul. Michalowskiego 12, 31-126 Krakow, Poland., Jaworek J; Department of Medical Physiology, Jagiellonian University Medical College, ul. Michalowskiego 12, 31-126 Krakow, Poland., Yang S; Department of Pathology, Johns Hopkins University, 400 N. Broadway Street Baltimore, Maryland 21287., Zhang H; Department of Pathology, Johns Hopkins University, 400 N. Broadway Street Baltimore, Maryland 21287., Kelly T; Mass Spec Core Facility, KBI Biopharma, 1101 Hamlin Road Durham, North Carolina 27704., Klapoetke S; Mass Spec Core Facility, KBI Biopharma, 1101 Hamlin Road Durham, North Carolina 27704., Cao R; Mass Spec Core Facility, KBI Biopharma, 1101 Hamlin Road Durham, North Carolina 27704., Kim JY; Division of Mass Spectrometry, Korea Basic Science Institute, 162 YeonGuDanji-Ro, Ochang-eup, Cheongwon-gu, Cheongju Chungbuk, 363-883 Korea (South)., Lee HK; Division of Mass Spectrometry, Korea Basic Science Institute, 162 YeonGuDanji-Ro, Ochang-eup, Cheongwon-gu, Cheongju Chungbuk, 363-883 Korea (South)., Lee JY; Division of Mass Spectrometry, Korea Basic Science Institute, 162 YeonGuDanji-Ro, Ochang-eup, Cheongwon-gu, Cheongju Chungbuk, 363-883 Korea (South)., Yoo JS; Division of Mass Spectrometry, Korea Basic Science Institute, 162 YeonGuDanji-Ro, Ochang-eup, Cheongwon-gu, Cheongju Chungbuk, 363-883 Korea (South)., Kim SR; Advanced Therapy Products Research Division, Korea National Institute of Food and Drug Safety, 187 Osongsaengmyeong 2-ro Osong-eup, Heungdeok-gu, Cheongju-si, Chungcheongbuk-do, 363-700, Korea (South)., Suh SK; Advanced Therapy Products Research Division, Korea National Institute of Food and Drug Safety, 187 Osongsaengmyeong 2-ro Osong-eup, Heungdeok-gu, Cheongju-si, Chungcheongbuk-do, 363-700, Korea (South)., de Haan N; Center for Proteomics and Metabolomics, Leiden University Medical Center, P.O. Box 9600, 2300 RC Leiden, The Netherlands., Falck D; Center for Proteomics and Metabolomics, Leiden University Medical Center, P.O. Box 9600, 2300 RC Leiden, The Netherlands., Lageveen-Kammeijer GSM; Center for Proteomics and Metabolomics, Leiden University Medical Center, P.O. Box 9600, 2300 RC Leiden, The Netherlands., Wuhrer M; Center for Proteomics and Metabolomics, Leiden University Medical Center, P.O. Box 9600, 2300 RC Leiden, The Netherlands., Emery RJ; Ludger Limited, Culham Science Centre, Abingdon, Oxfordshire, OX14 3EB, United Kingdom., Kozak RP; Ludger Limited, Culham Science Centre, Abingdon, Oxfordshire, OX14 3EB, United Kingdom., Liew LP; Ludger Limited, Culham Science Centre, Abingdon, Oxfordshire, OX14 3EB, United Kingdom., Royle L; Ludger Limited, Culham Science Centre, Abingdon, Oxfordshire, OX14 3EB, United Kingdom., Urbanowicz PA; Ludger Limited, Culham Science Centre, Abingdon, Oxfordshire, OX14 3EB, United Kingdom., Packer NH; Biomolecular Discovery and Design Research Centre and ARC Centre of Excellence for Nanoscale BioPhotonics (CNBP), Macquarie University, North Ryde, Australia., Song X; Biomolecular Discovery and Design Research Centre and ARC Centre of Excellence for Nanoscale BioPhotonics (CNBP), Macquarie University, North Ryde, Australia., Everest-Dass A; Biomolecular Discovery and Design Research Centre and ARC Centre of Excellence for Nanoscale BioPhotonics (CNBP), Macquarie University, North Ryde, Australia., Lattová E; Proteomics, Central European Institute for Technology, Masaryk University, Kamenice 5, A26, 625 00 BRNO, Czech Republic., Cajic S; Max Planck Institute for Dynamics of Complex Technical Systems, Sandtorstrasse 1, 39106 Magdeburg, Germany., Alagesan K; Department of Biomolecular Sciences, Max Planck Institute of Colloids and Interfaces, 14424 Potsdam, Germany., Kolarich D; Department of Biomolecular Sciences, Max Planck Institute of Colloids and Interfaces, 14424 Potsdam, Germany., Kasali T; AstraZeneca, Granta Park, Cambridgeshire, CB21 6GH United Kingdom., Lindo V; AstraZeneca, Granta Park, Cambridgeshire, CB21 6GH United Kingdom., Chen Y; Merck, 2015 Galloping Hill Rd, Kenilworth, New Jersey 07033., Goswami K; Merck, 2015 Galloping Hill Rd, Kenilworth, New Jersey 07033., Gau B; Analytical R&D, MilliporeSigma, 2909 Laclede Ave. St. Louis, Missouri 63103., Amunugama R; MS Bioworks, LLC, 3950 Varsity Drive Ann Arbor, Michigan 48108., Jones R; MS Bioworks, LLC, 3950 Varsity Drive Ann Arbor, Michigan 48108., Stroop CJM; MSD, Molenstraat 110, 5342 CC Oss, The Netherlands., Kato K; Exploratory Research Center on Life and Living Systems (ExCELLS), National Institutes of Natural Sciences, 5-1 Higashiyama, Myodaiji, Okazaki 444-8787 Japan; Graduate School of Pharmaceutical Sciences, Nagoya City University, 3-1 Tanabe-dori, Mizuhoku, Nagoya 467-8603 Japan., Yagi H; Graduate School of Pharmaceutical Sciences, Nagoya City University, 3-1 Tanabe-dori, Mizuhoku, Nagoya 467-8603 Japan., Kondo S; Graduate School of Pharmaceutical Sciences, Nagoya City University, 3-1 Tanabe-dori, Mizuhoku, Nagoya 467-8603 Japan; Medical & Biological Laboratories Co., Ltd, 2-22-8 Chikusa, Chikusa-ku, Nagoya 464-0858 Japan., Yuen CT; National Institute for Biological Standards and Control, Blanche Lane, South Mimms, Potters Bar, Hertfordshire EN6 3QG United Kingdom., Harazono A; Division of Biological Chemistry & Biologicals, National Institute of Health Sciences, 1-18-1 Kamiyoga, Setagaya-ku, Tokyo 158-8501 Japan., Shi X; New England Biolabs, Inc., 240 County Road, Ipswich, Massachusetts 01938., Magnelli PE; New England Biolabs, Inc., 240 County Road, Ipswich, Massachusetts 01938., Kasper BT; New York University, 100 Washington Square East New York City, New York 10003., Mahal L; New York University, 100 Washington Square East New York City, New York 10003., Harvey DJ; Target Discovery Institute, Nuffield Department of Medicine, University of Oxford, Roosevelt Drive, Oxford, OX3 7FZ, United Kingdom., O'Flaherty R; GlycoScience Group, The National Institute for Bioprocessing Research and Training, Fosters Avenue, Mount Merrion, Blackrock, Co. Dublin, Ireland., Rudd PM; GlycoScience Group, The National Institute for Bioprocessing Research and Training, Fosters Avenue, Mount Merrion, Blackrock, Co. Dublin, Ireland., Saldova R; GlycoScience Group, The National Institute for Bioprocessing Research and Training, Fosters Avenue, Mount Merrion, Blackrock, Co. Dublin, Ireland., Hecht ES; Department of Chemistry, North Carolina State University, 2620 Yarborough Drive Raleigh, North Carolina 27695., Muddiman DC; Department of Chemistry, North Carolina State University, 2620 Yarborough Drive Raleigh, North Carolina 27695., Kang J; Pantheon, 201 College Road East Princeton, New Jersey 08540., Bhoskar P; Pfizer Inc., 1 Burtt Road Andover, Massachusetts 01810., Menard D; Pfizer Inc., 1 Burtt Road Andover, Massachusetts 01810., Saati A; Pfizer Inc., 1 Burtt Road Andover, Massachusetts 01810., Merle C; Proteodynamics, ZI La Varenne 20-22 rue Henri et Gilberte Goudier 63200 RIOM, France., Mast S; ProZyme, Inc., 3832 Bay Center Place Hayward, California 94545., Tep S; ProZyme, Inc., 3832 Bay Center Place Hayward, California 94545., Truong J; ProZyme, Inc., 3832 Bay Center Place Hayward, California 94545., Nishikaze T; Koichi Tanaka Mass Spectrometry Research Laboratory, Shimadzu Corporation, 1 Nishinokyo Kuwabara-cho Nakagyo-ku, Kyoto, 604 8511 Japan., Sekiya S; Koichi Tanaka Mass Spectrometry Research Laboratory, Shimadzu Corporation, 1 Nishinokyo Kuwabara-cho Nakagyo-ku, Kyoto, 604 8511 Japan., Shafer A; Children's GMP LLC, St. Jude Children's Research Hospital, 262 Danny Thomas Place Memphis, Tennessee 38105., Funaoka S; Sumitomo Bakelite Co., Ltd., 1-5 Muromati 1-Chome, Nishiku, Kobe, 651-2241 Japan., Toyoda M; Sumitomo Bakelite Co., Ltd., 1-5 Muromati 1-Chome, Nishiku, Kobe, 651-2241 Japan., de Vreugd P; Synthon Biopharmaceuticals, Microweg 22 P.O. Box 7071, 6503 GN Nijmegen, The Netherlands., Caron C; Takeda Pharmaceuticals International Co., 40 Landsdowne Street Cambridge, Massachusetts 02139., Pradhan P; Takeda Pharmaceuticals International Co., 40 Landsdowne Street Cambridge, Massachusetts 02139., Tan NC; Takeda Pharmaceuticals International Co., 40 Landsdowne Street Cambridge, Massachusetts 02139., Mechref Y; Department of Chemistry and Biochemistry, Texas Tech University, 2500 Broadway, Lubbock, Texas 79409., Patil S; Thermo Fisher Scientific, 1214 Oakmead Parkway Sunnyvale, California 94085., Rohrer JS; Thermo Fisher Scientific, 1214 Oakmead Parkway Sunnyvale, California 94085., Chakrabarti R; United States Pharmacopeia India Pvt. Ltd. IKP Knowledge Park, Genome Valley, Shamirpet, Turkapally Village, Medchal District, Hyderabad 500 101 Telangana, India., Dadke D; United States Pharmacopeia India Pvt. Ltd. IKP Knowledge Park, Genome Valley, Shamirpet, Turkapally Village, Medchal District, Hyderabad 500 101 Telangana, India., Lahori M; United States Pharmacopeia India Pvt. Ltd. IKP Knowledge Park, Genome Valley, Shamirpet, Turkapally Village, Medchal District, Hyderabad 500 101 Telangana, India., Zou C; Alberta Glycomics Centre, University of Alberta, Edmonton, Alberta T6G 2G2 Canada; Department of Chemistry, University of Alberta, Edmonton, Alberta T6G 2G2 Canada., Cairo C; Alberta Glycomics Centre, University of Alberta, Edmonton, Alberta T6G 2G2 Canada; Department of Chemistry, University of Alberta, Edmonton, Alberta T6G 2G2 Canada., Reiz B; Department of Chemistry, University of Alberta, Edmonton, Alberta T6G 2G2 Canada., Whittal RM; Department of Chemistry, University of Alberta, Edmonton, Alberta T6G 2G2 Canada., Lebrilla CB; Department of Chemistry, University of California, One Shields Ave, Davis, California 95616., Wu L; Department of Chemistry, University of California, One Shields Ave, Davis, California 95616., Guttman A; Horváth Csaba Memorial Laboratory for Bioseparation Sciences, Research Center for Molecular Medicine, Doctoral School of Molecular Medicine, Faculty of Medicine, University of Debrecen, Debrecen, Egyetem ter 1, Hungary., Szigeti M; Horváth Csaba Memorial Laboratory for Bioseparation Sciences, Research Center for Molecular Medicine, Doctoral School of Molecular Medicine, Faculty of Medicine, University of Debrecen, Debrecen, Egyetem ter 1, Hungary; Translational Glycomics Research Group, Research Institute of Biomolecular and Chemical Engineering, University of Pannonia, Veszprem, Egyetem ut 10, Hungary., Kremkow BG; Delaware Biotechnology Institute, University of Delaware, 15 Innovation Way Newark, Delaware 19711., Lee KH; Delaware Biotechnology Institute, University of Delaware, 15 Innovation Way Newark, Delaware 19711., Sihlbom C; Proteomics Core Facility, University of Gothenburg, Medicinaregatan 1G SE 41390 Gothenburg, Sweden., Adamczyk B; Department of Medical Biochemistry and Cell Biology, University of Gothenburg, Institute of Biomedicine, Sahlgrenska Academy, Medicinaregatan 9A, Box 440, 405 30, Gothenburg, Sweden., Jin C; Department of Medical Biochemistry and Cell Biology, University of Gothenburg, Institute of Biomedicine, Sahlgrenska Academy, Medicinaregatan 9A, Box 440, 405 30, Gothenburg, Sweden., Karlsson NG; Department of Medical Biochemistry and Cell Biology, University of Gothenburg, Institute of Biomedicine, Sahlgrenska Academy, Medicinaregatan 9A, Box 440, 405 30, Gothenburg, Sweden., Örnros J; Department of Medical Biochemistry and Cell Biology, University of Gothenburg, Institute of Biomedicine, Sahlgrenska Academy, Medicinaregatan 9A, Box 440, 405 30, Gothenburg, Sweden., Larson G; Department of Clinical Chemistry and Transfusion Medicine, Sahlgrenska Academy at the University of Gothenburg, Bruna Straket 16, 41345 Gothenburg, Sweden., Nilsson J; Department of Clinical Chemistry and Transfusion Medicine, Sahlgrenska Academy at the University of Gothenburg, Bruna Straket 16, 41345 Gothenburg, Sweden., Meyer B; Department of Chemistry, University of Hamburg, Martin Luther King Pl. 6 20146 Hamburg, Germany., Wiegandt A; Department of Chemistry, University of Hamburg, Martin Luther King Pl. 6 20146 Hamburg, Germany., Komatsu E; Department of Chemistry, University of Manitoba, 144 Dysart Road, Winnipeg, Manitoba, Canada R3T 2N2., Perreault H; Department of Chemistry, University of Manitoba, 144 Dysart Road, Winnipeg, Manitoba, Canada R3T 2N2., Bodnar ED; Department of Chemistry, University of Manitoba, 144 Dysart Road, Winnipeg, Manitoba, Canada R3T 2N2; Agilent Technologies, Inc., 5301 Stevens Creek Blvd Santa Clara, California 95051., Said N; Laboratory of Mass Spectrometry of Interactions and Systems, University of Strasbourg, UMR Unistra-CNRS 7140, France., Francois YN; Laboratory of Mass Spectrometry of Interactions and Systems, University of Strasbourg, UMR Unistra-CNRS 7140, France., Leize-Wagner E; Laboratory of Mass Spectrometry of Interactions and Systems, University of Strasbourg, UMR Unistra-CNRS 7140, France., Maier S; Natural and Medical Sciences Institute, University of Tübingen, Markwiesenstraβe 55, 72770 Reutlingen, Germany., Zeck A; Natural and Medical Sciences Institute, University of Tübingen, Markwiesenstraβe 55, 72770 Reutlingen, Germany., Heck AJR; Bijvoet Center for Biomolecular Research and Utrecht Institute for Pharmaceutical Sciences, Utrecht University, Padualaan 8, 3584 CH Utrecht, The Netherlands., Yang Y; Bijvoet Center for Biomolecular Research and Utrecht Institute for Pharmaceutical Sciences, Utrecht University, Padualaan 8, 3584 CH Utrecht, The Netherlands., Haselberg R; Division of Bioanalytical Chemistry, Amsterdam Institute for Molecules, Medicines and Systems, Vrije Universiteit Amsterdam, de Boelelaan 1085, 1081 HV Amsterdam, The Netherlands., Yu YQ; Department of Chemistry, Waters Corporation, 34 Maple Street Milford, Massachusetts 01757., Alley W; Department of Chemistry, Waters Corporation, 34 Maple Street Milford, Massachusetts 01757., Leone JW; Zoetis, 333 Portage St. Kalamazoo, Michigan 49007., Yuan H; Zoetis, 333 Portage St. Kalamazoo, Michigan 49007., Stein SE; Mass Spectrometry Data Center, Biomolecular Measurement Division, Material Measurement Laboratory, National Institute of Standards and Technology, 100 Bureau Drive Gaithersburg, Maryland 20899.

Publikováno v: Molecular & cellular proteomics : MCP [Mol Cell Proteomics] 2020 Jan; Vol. 19 (1), pp. 11-30. Date of Electronic Publication: 2019 Oct 07.

Cross-Ring Fragmentation Patterns in the Tandem Mass Spectra of Underivatized Sialylated Oligosaccharides and Their Special Suitability for Spectrum Library Searching.

Autor: De Leoz MLA; Mass Spectrometry Data Center, National Institute of Standards & Technology, 100 Bureau Drive Stop 8362, Gaithersburg, MD, 20899, USA. lornadeleoz@gmail.com.; Agilent Technologies, Inc., 2500 Regency Parkway, Cary, NC, 27518, USA. lornadeleoz@gmail.com., Simón-Manso Y; Mass Spectrometry Data Center, National Institute of Standards & Technology, 100 Bureau Drive Stop 8362, Gaithersburg, MD, 20899, USA., Woods RJ; Complex Carbohydrate Research Center and Department of Biochemistry and Molecular Biology, University of Georgia, 315 Riverbend Road, Athens, GA, 30602, USA., Stein SE; Mass Spectrometry Data Center, National Institute of Standards & Technology, 100 Bureau Drive Stop 8362, Gaithersburg, MD, 20899, USA.

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