Zobrazeno 1 - 10
of 10
pro vyhledávání: '"David N. B. Mallen"'
Publikováno v:
Biological Mass Spectrometry. 9:162-173
A crude extract from an ergot fermentation broth has been examined by high-performance liquid chromatography mass spectrometry (LC/MS). The [M + 1]+ ions formed from the mixture under chemical ionization conditions have also been studied using B/E li
Publikováno v:
Biological Mass Spectrometry. 5:449-452
The mass spectra of three stable isotope derivatives are presented to confirm ion assignments in the spectrum of the methoxime, trimethylsilyl ether, methyl ester from 15-oxo-13,14-dihydrothromboxane B2.
Autor:
David M. Rackham, P.R. Shrubsall, David N. B. Mallen, S.R. Baker, Jane McKee Smith, S.E. Morgan, S.W. McKay, W.B. Jamieson, W.J. Ross
Publikováno v:
Journal of Chromatography A. 214:249-256
Publikováno v:
Biological Mass Spectrometry. 4:358-363
The mass spectra of eleven derivatives are presented to provide structural support for the recently discovered prostaglandin, 6-oxo-PGF1alpha, which we have isolated from incubations of arachidonic acid with ram seminal vesicles or released during is
Autor:
Julie M. Smith, David N. B. Mallen
Publikováno v:
Biological Mass Spectrometry. 9:125-129
Gas chromatography mass spectrometry was used to characterize compounds observed throughout the synthesis of a cis-fused 3′,4′-dichlorophenyl bicyclo-octane, a potential CNS acting drug substance. An ortho chloro-effect identified the isomeric 2
Autor:
David N. B. Mallen, Julie M. Smith
Publikováno v:
Biological Mass Spectrometry. 6:472-475
The mass spectral characteristics of a group of 1[(2-benzyl-4-thiazolyl)methyl]-4-phenylpiperazines are discussed, and the information used to determine the structure of an impurity, degradation product and aid the characterization of compounds synth
Electron impact induced fragmentations of 2-(2-nitroanilino)thiophens and Di(2-nitrophenyl)sulphides
Autor:
Julie M. Smith, David N. B. Mallen
Publikováno v:
Organic Mass Spectrometry. 14:171-176
A prominent ortho interaction occurs during the mass spectral fragmentation of di(2-nitrophenyl)sulphides. No such effects are observed for the corresponding ethers or 2-(2-nitroanilino)thiophens. Variation of aromatic substituents can dramatically a
Autor:
David M. Rackham, Anthony F. Cockerill, Norman J. A. Gutteridge, David J. Osborne, David N. B. Mallen
Publikováno v:
Biological Mass Spectrometry. 4:187-189
The relatively rapid formation of pyrazoline adducts is a serious side reaction in the esterification of 15-oxo-PGF2alpha with ethereal diazomethane under conditions used routinely in the chemical derivatization of prostaglandins.
Publikováno v:
Journal of Agricultural and Food Chemistry. 24:1223-1225
Autor:
Steven A. Westwood, David E. Games, Michael S. Lant, Brian J. Woodhall, D. K. Scott, W. J. Irwin, E. S. Zai, J. J. Burger, E. Tomlinson, I. M. Beaumont, L. F. Lloyd, Christine Eckers, David N. B. Mallen, Brian P. Swann, B. V. Fisher, R. B. Raja
Publikováno v:
Analytical Proceedings. 19:121