Zobrazeno 1 - 10
of 10
pro vyhledávání: '"David J. Calvert"'
Publikováno v:
Organic Magnetic Resonance. 12:583-586
The 13C NMR spectra of 20 polymethoxy- and/or methylenedioxyflavonols are reported. In key cases assignments have been made by examination of fully coupled spectra.
Publikováno v:
Organic Magnetic Resonance. 20:191-193
Vicinal coupling constants in the 1H and 13C NMR spectra of r-1,t-2,c-3,t-4-tetrachlorotetralin change with temperature and solvent in a manner better explained by conformational equilibration than by intramolecular or solvent-determined distortions.
Publikováno v:
Magnetic Resonance in Chemistry. 26:619-621
Spin–spin coupling between 14N and 13C nuclei is observed in NMR spectra of some quaternary ammonium compounds, including a series of heterocyclic cations. 1J values are in the range 2.2–4.2 Hz. Instances of coupling through two and three bonds a
Publikováno v:
Chemischer Informationsdienst. 16
Publikováno v:
Organic Magnetic Resonance. 11:213-214
Chemical shifts for tritons in ortho, meta and para positions in toluene have been determined using a 64 MHz tritium NMR spectrometer. The order of shift is meta>para>ortho, whereas the calculated shift order for protons is meta>ortho>para.
Publikováno v:
Australian Journal of Chemistry. 35:1615
The selectivity of tritium labelling of double bonds by partial hydrogenation of the acetylenic analogue on Lindlar catalyst is investigated by 3H and 13C n.m.r. Examples of both the secondary isotope effect on chemical shift and the usefulness of 3H
Autor:
Judith M. Brittain, Tony C. Jones, Paul A. Newman, David J. Calvert, Peter B. D. de la Mare, Joyce M. Waters, Hitomi Suzuki
Publikováno v:
Journal of the Chemical Society, Perkin Transactions 2. :247
X-Ray crystallographic analysis of 1,1,3,4-tetrachlorotetralin-2,2-diol has shown that this compound is the trans-isomer, which can be reversibly dehydrated to give trans-1,1,3,4-tetrachlorotetralin-2-one of previously unknown configuration, produced
Publikováno v:
Journal of the Chemical Society, Perkin Transactions 2. :255
The chlorinations of 1-methyl-2-naphthol, 1-bromo-2-naphthol,2,2′-dihydroxy-1,1′-dinaphthylemethane, and 6-t-butyl-2-naphthol with excess of chlorine in acetic acid give tetralin-2-ones analogous to that formed from 1-chloro-2-naphthol. 1,6-Di-t-
Publikováno v:
Journal of the Chemical Society, Perkin Transactions 2. :2005
The 13C n.m.r. spectra of cyclohexa-2,5-dienones produced by bromination or nitration of a variety of methyl-substituted phenols are reported. Most of the signals have been assigned with the assistance of selective decoupling. Correlations of chemica
Publikováno v:
Journal of the Chemical Society, Perkin Transactions 2. :1015
Details of the carbon-13 n.m.r. spectra of four 1,2,3,4-tetrachlorotetralins (naphthalene tetrachlorides) and of three 1,2,3,4-tetrachloro-2-methyltetralins are presented. Chemical shifts of the signals attributable to the individual alicyclic and ar