Výsledky vyhledávání - "Daniela Palano"

Scale-Up of Trisodium [(3β,5β,12α)-3-[[4(S)-4-[Bis[2-[bis[(carboxy-kO)methyl]amino-kN]ethyl]amino-kN]-4-(carboxy-kO)-1-oxobutyl]amino]-12-hydroxycholan-24-oato(6-)]gadolinate(3-)], a Gd(III) Complex under Development As a Contrast Agent for MRI Coronary Angiography

Autor: Daniela Palano, Massimo Visigalli, Pier Lucio Anelli, Giuseppe Manfredi, Marcella Murru, Luciano Lattuada, Marco Sipioni, Pierfrancesco Morosini, Marino Brocchetta

Publikováno v: Organic Process Research & Development. 13:739-746

Process chemistry involved in the discovery and development routes to trisodium [(3β,5β,12α)-3-[[4(S)-4-[bis[2-[bis[(carboxy-kO)methyl]amino-kN]ethyl]amino-kN]-4-(carboxy-kO)-1-oxobutyl]amino]-12-hydroxycholan-24-oato(6-)]gadolinate(3-)] (B22956/1

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::f307302d61d873ade756b0f2abf20f38
https://doi.org/10.1021/op900008a

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Conjugates of Gd(III) Complexes to Di- and Tri-hydroxy Substituted Cholanoic Acids: Regioselective Oxidation with Hydroxysteroid Dehydrogenases

Autor: Daniela Palano, P. Morosini, D. Sartore, Marino Brocchetta, L. Falcone, G. Carrea, P. Pasta, Pier Lucio Anelli

Publikováno v: Biocatalysis and Biotransformation. 20:29-34

The preparative-scale oxidation of Gd(III) complexes of ligands containing 7,12-dihydroxy and 12-hydroxy substituted cholanoic moieties to the corresponding 12-oxo derivatives was accomplished by means of 12 f -hydroxysteroid dehydrogenase. The e

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::8f33e73a557822fa32752d322e636aaa
https://doi.org/10.1080/10242420210150

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Thermodynamic and structural aspects of manganese(II) complexes with polyaminopolycarboxylic ligands based upon 1,4,7,10-tetraazacyclododecane (cyclen). Crystal structure of dimeric [MnL]2·2CH3OH containing the new ligand 1,4,7,10-tetraazacyclododecane-1,4-diacetate

Autor: Barbara Valtancoli, Pietro Losi, Patrizia Rossi, Palma Mariani, Antonio Bianchi, Paola Paoli, Daniela Palano, Claudia Giorgi, Luisella Calabi

Publikováno v: Journal of the Chemical Society, Dalton Transactions. :917-922

The formation of manganese(II) complexes with polyaminopolycarboxylic ligands based upon 1,4,7,10-tetraazacyclododecane (cyclen) has been studied in aqueous solution by means of potentiometric and microcalorimetric techniques affording log K, ΔH° a

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::4b8cf5b2f5f70ea3d8df2b59bb6ec6e7
https://doi.org/10.1039/b009242h

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Unexpected formation of acylformamidines by reaction of primary carboxamides with MeONa in DMF in the presence of CHCl3

Autor: Daniela Palano, Marino Brocchetta, Pier Lucio Anelli, Debora Copez, Massimo Visigalli, Paola Paoli

Publikováno v: Tetrahedron. 53:15827-15832

Dichlorocarbene, which is generated by reaction of CHCl3 with MeONa, is likely to chlorinate DMF to produce the Vilsmeier-Haack-Amold salt that, in the presence of excess MeONa, gives DMF dimethylacetal (2). This latter reacts with primary amides to

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::c1d124d3c5009be8b6e725ab27512850
https://doi.org/10.1016/s0040-4020(97)10041-2

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ChemInform Abstract: Mild Conversion of Primary Carboxamides into Carboxylic Esters

Autor: Pier Lucio Anelli, Marino Brocchetta, Massimo Visigalli, Daniela Palano

Publikováno v: ChemInform. 28

Primary carboxamides are converted into the corresponding alkyl carboxylates by treatment with dimethylformamide dimethylacetal in the appropriate alcohol at 25–45 °C. Yields are very good to excellent.

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::2a228a533a3e0c56afd096ee403e1206
https://doi.org/10.1002/chin.199730061

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