Zobrazeno 1 - 10
of 233
pro vyhledávání: '"Clifton E. F. Rickard"'
Publikováno v:
Acta Crystallographica Section E, Vol 64, Iss 7, Pp m917-m918 (2008)
The cationic complex in the structure of the title compound, [Co(Et2NCS2)2(C12H8N2)]BF4, has a CoIII atom with a distorted octahedral coordination formed by four S atoms of two diethyldithiocarbamate and two N atoms of 1,10-phenanthroline ligands. Th
Externí odkaz:
https://doaj.org/article/90ea7103a123445d9090eea196433a82
Publikováno v:
Polyhedron. 30:632-637
Reaction of PhCONH2 with [WCl6] under reflux in benzene gives a near quantitative yield of [WOCl4(NCPh)] (1) which can be prepared directly by the reaction of PhCN and [WOCl4]. PhCONH2 reacts with [WOCl4] under reflux in benzene to give [WO2Cl2(NCPh)
Publikováno v:
Polyhedron. 29:1279-1284
A compound with a linear trinuclear copper(II) cation, [Cu3(μ-protan)2](ClO4)2·H2O (protanH2 = 3,7-bis(3-hydroxypropyl)-1,3,5,7-tetraazabicyclo[3,3,1]-nonane) is formed by reaction of copper(II) perchlorate, 3-aminopropanol, ammonia and methanal. T
Publikováno v:
Polyhedron. 28:739-748
The structure of the crystalline azamacrocyclic product formed by reaction of bis(propane-1,3-diamine)copper(II) perchlorate with acetone has been determined as N-rac -(6,8,8,14,16,16-hexamethyl-1,5,9,13-tetraazacyclohexadeca-5,13-diene)copper(II) ·
Autor:
Clifton E. F. Rickard, Michael M. Möhlen, Warren R. Roper, L. James Wright, George R. Whittell
Publikováno v:
Inorganica Chimica Acta. 360:1287-1297
Reaction between Os(SnI3)(κ2-S2CNMe2)(CO)(PPh3)2 and NaBH4 produces the unusual, air-stable, trihydridostannyl complex, Os(SnH3)(κ2-S2CNMe2)(CO)(PPh3)2 (1), which has been fully characterised including by X-ray crystal structure determination.Simil
Autor:
Warren R. Roper, L. James Wright, George R. Whittell, Clifton E. F. Rickard, Michael M. Möhlen
Publikováno v:
Journal of Organometallic Chemistry. 691:4065-4075
Reaction between Os(SnClMe2)(κ2-S2CNMe2)(CO)(PPh3)2 and either LiSnMe3 or KSnPh3 produces the distannyl complexes, Os(SnMe2SnMe3)(κ2-S2CNMe2)(CO)(PPh3)2 (1) or Os(SnMe2SnPh3)(κ2-S2CNMe2)(CO)(PPh3)2 (3), respectively. Similarly, reaction between Os
Publikováno v:
Journal of Organometallic Chemistry. 691:2593-2598
Treatment of Os(κ 2 -S 2 CNMe 2 )H(CO)(PPh 3 ) 2 with HSiMeCl 2 or HSiCl 3 gives in high yield Os(κ 2 -S 2 CNMe 2 )(SiMeCl 2 )(CO)(PPh 3 ) 2 ( 1 ) or Os(κ 2 -S 2 CNMe 2 )(SiCl 3 )(CO)(PPh 3 ) 2 ( 2 ), respectively. The crystal structures of both c
Publikováno v:
Polyhedron. 24:3022-3031
The imine functions of [Ni(mL1)](ClO4)2 (mL1 = meso-7RS,14SR-5,12-dimethyl-7,14-diphenyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene) are reduced by using NaBH4 in acetonitrile/methanol to form the meso–meso and rac–meso isomeric cyclic tetramine
Publikováno v:
Inorganica Chimica Acta. 358:4145-4155
Treatment of the six-coordinate trimethylstannyl complex, Os(SnMe3)(κ2-S2CNMe2)(CO)(PPh3)2 (1) with SnMe2Cl2 produces Os(SnMe2Cl)(κ2-S2CNMe2)(CO)(PPh3)2 (2), which in turn reacts readily with hydroxide ion to give, Os(SnMe2OH)(κ2-S2CNMe2)(CO)(PPh3
Publikováno v:
Journal of Organometallic Chemistry. 690:4114-4123
Heating the five-coordinate trimethylstannyl complex, Os(SnMe3)Cl(CO)(PPh3)2, in solution with triphenylphosphine induces an ortho-stannylation of one phenyl group of a triphenylphosphine ligand and an ortho-metallation of another triphenylphosphine