Zobrazeno 1 - 10
of 11
pro vyhledávání: '"Charles W. Moeder"'
Publikováno v:
Journal of Liquid Chromatography & Related Technologies. 28:3131-3142
Trifluorophenylacetic acid (TFPAA) was synthesized from 2,4,5‐trifluorophenyl bromide and malonic acid starting materials as part of process development for a pharmaceutical intermediate. Impurity profile methods, sensitive to positional isomers, h
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::adf75c80618c6ea899c77a11fa4adc3b
https://doi.org/10.1080/10826070500295278
https://doi.org/10.1080/10826070500295278
Autor:
Michelle Hardiman, Gerri Hutson, Daniel J. Kumke, Charles W. Moeder, David A. Conlon, Laura Sailer
Publikováno v:
Advanced Synthesis & Catalysis. 346:1307-1315
Addition of methylmagnesium chloride to ester 1 in the presence of cerium chloride gave significantly better yields of the tertiary alcohol 2 than the reaction performed in the absence of cerium chloride. The beneficial effect of added cerium chlorid
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::dc59b39d690de3686a34f0d726c0b62d
https://doi.org/10.1002/adsc.200404075
https://doi.org/10.1002/adsc.200404075
Autor:
Charles W. Moeder, John R. Sowa
Publikováno v:
Journal of Physical Organic Chemistry. 17:317-324
A quantitative investigation was undertaken to determine experimentally the relative reaction rates of the heterochiral and homochiral species of B-chlorodiisopinocampheylborane (Dip-Cl), a reagent that exhibits asymmetric amplification. Using the me
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::1476784d86ad644f65edbbfe3889e6e0
https://doi.org/10.1002/poc.730
https://doi.org/10.1002/poc.730
Publikováno v:
Journal of the American Chemical Society. 122:7218-7225
We show that complexation of B-chlorodiisopinocampheylborane (Dip-Cl) with 8-hydroxyquinoline results in an air- and moisture-stable complex. Using enantiomerically pure (+)-α-pinene, the (+,+)-Dip-quinoline complex, [(+)-C10H17]2B(η2-N,O-C10H6NO),
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::1d37d5ba8105fcb87080896a12f4be7a
https://doi.org/10.1021/ja000158j
https://doi.org/10.1021/ja000158j
Publikováno v:
Journal of Pharmaceutical and Biomedical Analysis. 19:327-333
We report the determination of residual bis(tributyltin) oxide in a drug substance by GC-MS after extraction and on-line conversion to tributyltin hydride. Gas chromatography was performed using a 15 m x 0.25 mm i.d. DB-5 HT column with a temperature
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::976d91e8f1de502d636684cd6b896e0c
https://doi.org/10.1016/s0731-7085(98)00125-3
https://doi.org/10.1016/s0731-7085(98)00125-3
Autor:
John O. Egekeze, Charles W. Moeder, G. Bicker, Robert D. Larsen, Anthony O. King, James D. Carroll, Holly J. Perpall
Publikováno v:
The Analyst. 122:1353-1358
A reversed-phase HPLC method has been developed for the determination of vinylmagnesium chloride and vinylmagnesium bromide, based on the assay of 1-(9-anthryl)propen-2-ol, the product in the reaction between a vinylmagnesium halide and 9-anthraldehy
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::8e342abd28d6214ccfda8af48ba05428
https://doi.org/10.1039/a701513e
https://doi.org/10.1039/a701513e
Autor:
Holly J. Perpall, Richard Thompson, T. Loughlin, Charles W. Moeder, G.B. Smith, G. Bicker, Nelu Grinberg, M. Bhupathy, K. Chong
Publikováno v:
Journal of Pharmaceutical and Biomedical Analysis. 15:111-121
Effective process control can only be achieved through an understanding of the operating issues of the reaction. The development and use of effective and rugged analytical methods is necessary to monitor these parameters. The intent of this paper is
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::a5de752a2fb21b5aecae2f6e29cf6fb5
https://doi.org/10.1016/0731-7085(96)01810-9
https://doi.org/10.1016/0731-7085(96)01810-9
Publikováno v:
Journal of Chromatography A. 736:1-9
The stoichiometric coefficients and apparent formation constants for (±)- α -pinene, (±)- β -pinene, (±)-camphene and (±)-limonene with α- and β-cyclodextrins were determined using high-performance liquid chromatography. These measurements we
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::9e4e601211b96c16d44bec47f351bc31
https://doi.org/10.1016/0021-9673(95)01276-1
https://doi.org/10.1016/0021-9673(95)01276-1
Autor:
Toma Ph, Charles W. Moeder, Louis S. Crocker, Conlon Da, Nelu Grinberg, Richard Thompson, Karen C. Thompson, Thomas P. O'Brien, Binyamin Feibush, G. Bicker
Publikováno v:
Analytical chemistry. 69(11)
Cellulose and cellulose derivatives are biopolymers which are often used as stationary phases for the separation of enantiomers. Describing the mechanism of such separations is a difficult task due to the complexity of these phases. In the present st
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::0b2d4b4bf6f71f36e9cfa3346f1e0c63
https://pubmed.ncbi.nlm.nih.gov/21639239
https://pubmed.ncbi.nlm.nih.gov/21639239
Autor:
Charles W. Moeder, John R. Sowa
Publikováno v:
Journal of Physical Organic Chemistry; Apr2004, Vol. 17 Issue 4, p317-324, 8p