Výsledky vyhledávání - "Brigida Allieri"

Application of the Quality by Design Principles for the Development of the Crystallization Process for a Piperazinyl-Quinoline and Definition of the Control Strategy for Form 1

Autor: Sara Rossi, Davide Tramarin, William Maton, Brigida Allieri, Francesca Campi, Pieter Westerduin, Gilles Laval, Jason W. B. Cooke, Zadeo Cimarosti, Paolo Stabile, Nicola Giubellina

Publikováno v: Organic Process Research & Development. 16:1598-1606

The studies carried out to develop a robust crystallization method for the substituted piperazinyl-quinoline (1) a compound potentially active in the treatment of depression, are described in this contribution. These studies include the control of a

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::7047d1fcd161eb000d8b634507416017
https://doi.org/10.1021/op300126e

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Kinetic performance of reversed-phase C18 high-performance liquid chromatography columns compared by means of the Kinetic Plot Method in pharmaceutically relevant applications

Autor: Guido Bellazzi, Brigida Allieri, Alessandro Rottigni, Gert Desmet, Deirdre Cabooter, A. Fanigliulo

Publikováno v: Journal of Chromatography A. 1218:3351-3359

Four fully porous C18 columns (Hypersil Gold, ACE3, Xbridge and Gemini NX), widely employed in the pharmaceutical industry, were compared in terms of efficiency and analysis speed with the Kinetic Plot Method. Weakly basic, medium-sized, N-containing

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::779e8c01564317f3ff807a88308a0f9f
https://doi.org/10.1016/j.chroma.2010.08.071

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Comparison of performance of high-performance liquid chromatography columns packed with superficially and fully porous 2.5 μm particles using kinetic plots

Autor: Alessandro Rottigni, A. Fanigliulo, Brigida Allieri, Gert Desmet, Deirdre Cabooter, Davide Tramarin, Guido Bellazzi

Publikováno v: Journal of Separation Science. 33:3655-3665

A recently introduced 2.5 μm fully porous support (Kromasil Eternity) is compared with three different brands of superficially porous material (Kinetex, Halo and Poroshell 120) by means of the kinetic plot method using pharmaceutical compounds from

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_________::6e614e3578cf2394b51f1f12cf6c2787
https://doi.org/10.1002/jssc.201000463

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Relationship between the particle size distribution of commercial fully porous and superficially porous high-performance liquid chromatography column packings and their chromatographic performance

Autor: Alessandro Rottigni, Gert Desmet, Guido Bellazzi, A. Fanigliulo, Brigida Allieri, Deirdre Cabooter

Publikováno v: Vrije Universiteit Brussel

The separation efficiency and kinetics of several commercial HPLC particle types (both fully porous and superficially porous) have been investigated using a pharmaceutical weakly basic N-containing compound as a test molecule. A strong trend between

Externí odkaz: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::83b267503bf17ac2013d2d437ac7f147
https://pubmed.ncbi.nlm.nih.gov/20870241

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