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Autor:
Thomas J. Thamann, Jane E. Guido, Bowman Phil B, Kathleen A. Farley, Frank W. Crow, Brenda S. Vonderwell, Russell H. Robins, Gary E. Martin, Richard F. Smith, Wayne K. Duholke, Sandra M. Sims, Jay C. Brumfield
Publikováno v:
Magnetic Resonance in Chemistry. 36:S11-S16
A method is described for unequivocally establishing the site of N-oxidation which relies on the relatively large downfield shift of aliphatic nitrogen resonances following oxidation. The technique described is based on 15N at natural abundance and d