Zobrazeno 1 - 10
of 17
pro vyhledávání: '"Bart H. Wouters"'
Autor:
A. Goossens, V. Buschmann, Lucien Fiermans, Bart H. Wouters, Johan A. Martens, Piet J. Grobet
Publikováno v:
European Journal of Inorganic Chemistry. 2001:1167-1181
Epitaxial FAU zeolite films were achieved on micrometer-sized EMT support crystals using a two-step synthetic procedure, in which EMT support crystals with hexagonal-platelet morphology, were added to a synthesis gel for the crystallization of an FAU
Publikováno v:
Microporous and Mesoporous Materials. :453-457
Two solid-state NMR methods are proposed to study the degree of silylation of MCM-41 with trimethylchlorosilane (TMCS). Both 29 Si MAS NMR and 1 H MAS NMR provide an accurate estimation of the amount of trimethylsilane attached to MCM-41. A silylatio
Publikováno v:
The Journal of Physical Chemistry B. 105:1135-1139
Steamed zeolite Y samples were examined by 27Al MAS NMR, 1H spin−echo editing MAS NMR, and 1H27Al} double-resonance MAS NMR in order to evaluate the dealumination process during steaming. Framework...
Autor:
Pierre Jacobs, Piet J. Grobet, Bart H. Wouters, Eddy J. P. Feijen, A. Goossens, Johan A. Martens, Guy Verhoeven
Publikováno v:
Microporous and Mesoporous Materials. :555-572
An attempt was made to synthesize MAZ-type zeolites with enhanced Si/Al ratio by adding organic molecules to conventional aluminosilicate hydrogels for MAZ zeolites containing sodium and tetramethylammonium cations. Molecular models of candidate temp
Publikováno v:
European Journal of Inorganic Chemistry. 2000:281-285
27Al 3Q MAS NMR spectroscopy has been applied to study the coordination state of the species giving the 30 ppm Al NMR signal in the 27Al MAS NMR spectrum of activated mordenite materials. From the 27Al 3Q MAS NMR measurements it is evident that the b
Publikováno v:
Colloids and Surfaces A: Physicochemical and Engineering Aspects. 158:145-149
The Al coordination state of molecular sieve SAPO-37 has been studied by 27 Al multiple quantum (MQ) MAS NMR spectroscopy. Although the 1D 27 Al MAS NMR spectrum of the aluminum sites show a complex pattern, the 3Q MAS NMR spectra of SAPO-37, submitt
Publikováno v:
The Journal of Physical Chemistry B. 103:8093-8096
The MQ MAS NMR is used to evaluate the real, individual line shape of the Al signals in the 1D 27Al MAS NMR spectrum of zeolite materials. By the application of these real line shapes, an improved deconvolution of the 1D MAS NMR spectrum is achieved.
Publikováno v:
The Journal of Physical Chemistry B. 103:6179-6184
The aluminum coordination state of the molecular sieve SAPO-37 has been studied by 27Al multiple quantum (MQ) magic angle spinning (MAS) NMR spectroscopy. Although the 1D 27Al MAS NMR spectra of the aluminum sites show complex patterns, the 2D 3Q MAS
Publikováno v:
Advanced Materials. 11:561-564
Autor:
Dirk De Vos, Piet J. Grobet, L.K.M Van Looveren, Ivo F.J. Vankelecom, Bart H. Wouters, P.A. Jacobs
Publikováno v:
Applied Catalysis A: General. 180:L5-L10
The in situ synthesis of methylalumoxane (MAO) on the crystalline structure of heteropoly acids generates a highly active and weakly coordinating compound for the metallocene catalyst. The MAO-phase formed by the controlled hydrolysis of trimethylalu