Zobrazeno 1 - 10
of 126
pro vyhledávání: '"Anne Irving"'
Autor:
Anne Irving, Harry M. N. H. Irving
Publikováno v:
Journal of Chemical Crystallography. 24:251-257
C12H3Cl6O4, (I),Mr=428.91, triclinic,\(P\bar 1\),a=9.197(1),b=9.336(2),c=9.830(1) A, α=79.29(1), β=83.33(1), γ=85.38(1)°,V=822.16,Z=2,Dx=1.73 Mg m−3,F(000)=428, λ(MoKα)=0.71069 A, μ=10.62 cm−1, room temperature, finalR=0.033 for 2573 uniqu
Publikováno v:
Journal of Chemical Crystallography. 24:267-271
The host compound forms a coordinato-clathrate in a coordination assisted host lattice. The host lattice is provided by hydrogen bonding between the nitrogen atom of the cyano group and two hydrogen atoms from the phosphonium methyl group. Guest mole
Publikováno v:
Angewandte Chemie. 106:588-591
Autor:
Anne Irving, Harry M. N. H. Irving
Publikováno v:
Journal of Crystallographic and Spectroscopic Research. 23:725-731
The title compound is monoclinic,P21/n,Z=4,a=9.934(1),b=18.399(2),c=11.098(2)A, β=111.08(1)°. The molecule can conveniently be visualized as a benzophenone molecule with one of the aromatic rings fused to a 1,3-dioxin ring which adopts a distorted
Autor:
Anne Irving
Publikováno v:
Journal of Crystallographic and Spectroscopic Research. 23:733-738
Crystals of the title compound are monoclinic,P21,a=9.791(4),b=7.129(3),c=10.428(3)A,β=91.84(3)°,V=727.50A3,Z=2. The structure was solved by direct methods, from data collected at room temperature on an Enraf-Nonius CAD4 diffractometer, and refined
Publikováno v:
Inorganica Chimica Acta. 206:193-199
N,N-Di(n-butyl)-N′-benzoylthiourea readily reacts with PtX42− to yield neutral cis-[PtL2] complexes for X = Cl− and Br−, while for X = I−, the protonated cis-[Pt(LH)2]I2 complex is isolated. The crystal structure of cis-[PtL2] is reported.
Publikováno v:
Journal of Organometallic Chemistry. 443:232-240
The mononuclear cobaloxime complex o -[{(py)(DH) 2 CoCH 2 }C 6 H 4 (CH 2 Br)] ( 1 ) has been prepared by the reaction of the appropriate xylene dibromide with an equimolar amount of [Co(DH) 2 (py)Cl] in the presence of sodium borohydride (where DH =
Autor:
Anne Irving
Publikováno v:
Journal of Crystallographic and Spectroscopic Research. 22:533-540
8-Acetylamino-6-methyl-2,4-bis(trichloromethyl)-1,3-benzdioxin, (I), is monoclinic,P21/c,a=15.174(4),b=11.977(7),c=9.911(3)A,β=99.72(2)°. 6-Acetylamino-2,4-bis(trichloromethyl)-1,3-benzdioxin, (II), is monoclinic,P21/n,a=5.927(4),b=40.623(1),c =7.1
Autor:
Harry M. N. H. Irving, Anne Irving
Publikováno v:
Acta Crystallographica Section C Crystal Structure Communications. 48:88-91
Methyl-2,4-bis(trichloromethyl)- 1,3-ben- zodioxin-8-carboxylic acid and its methyl and ethyl esters have been prepared. For the methyl ester C13HloC1604, 34, = 442.94, triclinic, P1, a =
Autor:
Anne Irving, Harry M. N. H. Irving
Publikováno v:
Journal of Crystallographic and Spectroscopic Research. 21:479-483
The condensation ofp-nitrothiophenol with formaldehyde and with trichloroacetaldehyde is described. 2,2-Bis(4′-nitro-1′-mercaptophenyl)-1,1,1-trichloroethane is monoclinic,P21/c,a=7.717(2),b=34.666(5),c=7.258(1) (A),β=116.32 (1) (deg.),V=1740.35