Zobrazeno 1 - 10
of 122
pro vyhledávání: '"Andrzej Sygula"'
Autor:
Steven F. Watkins, Frank R. Fronczek, Peter W. Rabideau, Andrzej Sygula, Gregory T. McCandless
Publikováno v:
Acta Crystallographica Section E, Vol 68, Iss 5, Pp o1458-o1459 (2012)
The title compound, C36H24O6·CH2Cl2, is a dimer of two essentially planar (r.m.s., deviations of fitted plane of 14 pyracene C atoms = 0.0539 and 0.0543 Å) tetracyclic pyracene frameworks (each with four methyl groups and three carbonyl groups on t
Externí odkaz:
https://doaj.org/article/fc9b6df50b4141fe8634e27e74c951e8
Autor:
Andrzej Sygula, Behzad Farajidizaji, Karl M. Mukeba, Charles U. Pittman, Dennis W. Smith, Ganesh Narayanan, Ketki E. Shelar, Bruno Donnadieu
Publikováno v:
Journal of Polymer Science Part A: Polymer Chemistry. 57:1270-1274
Autor:
Dongmao Zhang, Xue Xu, Charles Edwin Webster, Bassem Ahmed, Andrzej Sygula, Xin Cui, Hetti Handi Chaminda Lakmal, Christopher Fong, David J. Szalda, Joanna Xiuzhu Xu, Keith Ramig
Publikováno v:
The Journal of Organic Chemistry. 83:9497-9503
C-Unsubstituted 1,2-diazetidines, a rarely studied type of four-membered heterocyclic compounds, were synthesized through an operationally simple intermolecular vicinal disubstitution reaction. 1,2-Diazetidine derivatives bearing various N-arylsulfon
Autor:
Andrzej Sygula
Publikováno v:
Synlett. 27:2070-2080
This brief review outlines recent developments in synthetic methodologies leading to the preparation of efficient molecular receptors for binding fullerenes via the concave–convex π–π stacking of the carbon cages with the corannulene pincers. A
Publikováno v:
Organic Letters. 18:3054-3057
Bis-corannulenoanthracene (C50H22, 5) was prepared by the Diels-Alder double cycloaddition of isocorannulenofuran with "bis-benzyne", followed by deoxygenation of the adducts. Despite the presence of a pentacene core, 5 is stable enough to be isolate
Publikováno v:
The Journal of Physical Chemistry. B
(1)H NMR and isothermal titration calorimetry (ITC) experiments were employed to obtain reliable thermodynamic data for the formation of the 1:1 inclusion complexes of fullerenes C(60) and C(70) with the buckycatcher (C(60)H(28)). NMR measurements we
Publikováno v:
Journal of Chemical Education. 91:2186-2190
This laboratory exercise introduces undergraduate chemistry majors to the spectroscopic and theoretical study of the polycyclic aromatic hydrocarbon (PAH), corannulene. Students explore the spectroscopic properties of corannulene using UV–vis and R
Autor:
Frank R. Fronczek, Alexander V. Zabula, Marina A. Petrukhina, William P. Henry, Michael Yanney, Andrzej Sygula
Publikováno v:
Crystal Growth & Design. 14:2633-2639
X-ray crystal structure study of cocrystallites of buckycatcher (2, C60H28) demonstrates a remarkable versatility of the molecular clip to accommodate guest molecules of various sizes and shapes. As demonstrated by the B97-D calculations, concave–c
Autor:
Michael Yanney, Andrzej Sygula
Publikováno v:
Tetrahedron Letters. 54:2604-2607
A molecular clip 3 (C 87 H 54 O 6 ) with cyclotriveratrylene tether and three corannulene pincers was synthesized and tested for its affinity toward fullerenes. 1 H NMR titration experiment in toluene- d 8 suggests the formation of 1:1 fullerene@ 3 c