Zobrazeno 1 - 10
of 36
pro vyhledávání: '"Andrew C. Jupe"'
Publikováno v:
Cement and Concrete Research. 42:1083-1087
The hydration of tricalcium silicate (C{sub 3}S) is accelerated by pressure. However, the extent to which temperature and/or cement additives modify this effect is largely unknown. Time-resolved synchrotron powder diffraction has been used to study c
Publikováno v:
Cement and Concrete Research. 42:1166-1173
A sample cell for the simultaneous measurement of synchrotron X-ray powder diffraction and ultrasound shear-wave reflection data from cement slurries is described. White cement slurries at 25 and 50 C with 0-3% bwoc CaCl{sub 2} were studied to illust
Autor:
Peter J. Chupas, Benjamin K. Greve, Karena W. Chapman, Andrew C. Jupe, Angus P. Wilkinson, C. Kurtz, Cody R. Morelock
Publikováno v:
Journal of Applied Crystallography. 44:1047-1053
A collimator and beam-stop assembly that can be inserted inside a temperature-controlled pressure vessel, to reduce dramatically the parasitic Bragg scattering from the vessel, has been designed and evaluated. High-energy X-ray powder diffraction dat
Publikováno v:
Journal of the American Ceramic Society. 94:1591-1597
The hydration kinetics of a white cement and batches of both Class G and H oil-well cements were examined between 0 and 60 MPa, at ≤80°C, using in situ synchrotron X-ray diffraction. This gives a continuous measure of the C3S (Ca3SiO5), CH (Ca(OH)
Autor:
William A. Bassett, Angus P. Wilkinson, Andrew C. Jupe, Karena W. Chapman, Peter L. Lee, E. A. Payzant, C.-S. Zha, K. M. White, Peter J. Chupas
Publikováno v:
Chemistry of Materials. 20:3728-3734
CeP2O7, a close structural relative of ZrP2O7, and many other MIVX2O7 (X – P, V, As) phases, forms on heating Ce(HPO4)2·xH2O between ∼300 and 600 °C and decomposes by oxygen loss at higher temperatures. In-situ X-ray diffraction measurements sh
Publikováno v:
Cement and Concrete Research. 38:660-666
Under deep oil-well conditions of elevated temperature and pressure, crystalline calcium silicate hydrates are formed during Portland cement hydration. The use of silica rich mineral additives leads to the formation of crystalline hydrates with bette
Publikováno v:
Journal of the American Ceramic Society. 90:2595-2602
Class A and H oil well cements are compared at 25 and 50 C with 0%, 1%, 2%, and 4% CaCl{sub 2}. Up to 4% CaCl{sub 2} accelerated Class A thickening, but 4% led to slower thickening than 2% for Class H. C{sub 3}S hydration in the two cements responded
Autor:
Andrew C. Jupe, Kimberly E. Kurtis, Stuart R. Stock, Angus P. Wilkinson, N. N. Naik, Peter L. Lee
Publikováno v:
Cement and Concrete Research. 36:144-159
X-ray microtomography (microCT) and spatially resolved energy dispersive X-ray diffraction (EDXRD) were used in combination to non-destructively monitor the physical and chemical manifestations of damage in Portland cement paste samples subjected to
Autor:
Andrew C. Jupe, Christopher Hall, Nicola Meller, S. L. Colston, John Dransfield, Paul Livesey, Simon D. M. Jacques, Paul Barnes, Geoffrey C. Maitland
Publikováno v:
Cement and Concrete Research. 35:2223-2232
The technique of synchrotron energy dispersive diffraction (EDD) has been developed for in situ studies of cement hydration under autoclave conditions. This has been applied to oilwell cements hydrating at typical oilwell temperatures up to 130 deg C
Publikováno v:
Industrial & Engineering Chemistry Research. 44:5579-5584
In situ powder X-ray diffraction was used to examine the hydration of API Class H cement slurries, with a water-to-cement ratio of 0.394, at 66, 93, 121, and 177 C under autogenous pressure in the presence of varying amounts of the additives tartaric