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Autor:
Anastasiya Yu. Kharintseva, Kseniya А. Stepanova, Dmitry N. Babentsev, Anastasiya E. Simakhina, Maksim V. Dmitriev, Vladimir А. Glushkov
Publikováno v:
Chemistry of Heterocyclic Compounds. 57:63-68
4-Aryl-2-methylbutan-2-ols with methoxy or methylenedioxy substituents participate in the Graf–Ritter reaction with methyl thiocyanate in the presence of an acid (H2SO4, MeSO3H) forming 1-methylsulfanyl-2-benzazepines in low yields (11–35%), whic