Zobrazeno 1 - 10
of 18
pro vyhledávání: '"Ana A. Folgueiras‐Amador"'
Publikováno v:
Beilstein Journal of Organic Chemistry, Vol 18, Iss 1, Pp 979-990 (2022)
In this paper we present the first electrochemical generation of NHC carried out in a divided flow cell. The flow cell operated in the recycle mode. The need for a divided cell derived from the anodic electroactivity of the electrogenerated carbene.
Externí odkaz:
https://doaj.org/article/7f8ab1dd6a08446c9dea6d9c6dfdee1b
Autor:
Ana A. Folgueiras-Amador, Katie E. Jolley, Peter R. Birkin, Richard C.D. Brown, Derek Pletcher, Stephen Pickering, Medhat Sharabi, Oscar de Frutos, Carlos Mateos, Juan A. Rincón
Publikováno v:
Electrochemistry Communications, Vol 100, Iss , Pp 6-10 (2019)
It is demonstrated that the addition of a non-ionic surfactant (Triton X-100 or Brij L23) to the electrolyte medium leads to a significant improvement to the current efficiency for the methoxylation of N-formylpyrrolidine in a flow electrolysis cell
Externí odkaz:
https://doaj.org/article/a52aadf3b9774043aac1482fc720b312
Autor:
Ana A. Folgueiras‐Amador, Alexander E. Teuten, Mateo Salam‐Perez, James E. Pearce, Guy Denuault, Derek Pletcher, Philip J. Parsons, David C. Harrowven, Richard C. D. Brown
Publikováno v:
Angewandte Chemie (International ed. in English). 61(35)
Electro-reductive radical cyclisation of aryl halides affords the corresponding hetero- and carbo-cycles in an undivided flow reactor equipped with steel and carbon electrodes using an organic mediator. A dissolving metal anode is not needed, and the
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::2e63c3c1dff67b4024f0e3797174f27e
https://pubmed.ncbi.nlm.nih.gov/35790060
https://pubmed.ncbi.nlm.nih.gov/35790060
Autor:
Jie Ke, Chuang Gao, Ana A. Folgueiras-Amador, Katherine E. Jolley, Oscar de Frutos, Carlos Mateos, Juan A. Rincón, Richard C. D. Brown, Martyn Poliakoff, Michael W. George
Publikováno v:
Applied spectroscopy. 76(1)
A continuous-flow electrochemical synthesis platform has been developed to enable self-optimization of reaction conditions of organic electrochemical reactions using attenuated total reflection Fourier transform infrared spectroscopy (ATR FT-IR) and
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::72053f957c97d36f112f42f3753865f1
https://pubmed.ncbi.nlm.nih.gov/34911387
https://pubmed.ncbi.nlm.nih.gov/34911387
Autor:
Diego E. Collin, Bruno Linclau, Richard C. D. Brown, Derek Pletcher, Mark E. Light, Ana A. Folgueiras-Amador
Publikováno v:
Chemistry (Weinheim an Der Bergstrasse, Germany)
The highly strained cubane system is of great interest as a scaffold and rigid linker in both pharmaceutical and materials chemistry. The first electrochemical functionalisation of cubane by oxidative decarboxylative ether formation (Hofer–Moest re
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::edd51eac8383b4c6a418b22a351f152a
https://doi.org/10.1002/chem.201904479
https://doi.org/10.1002/chem.201904479
Autor:
Thomas Wirth, Célina Génot, Ana A. Folgueiras-Amador, Haifa Alharbi, Mohamed Elsherbini, Bethan Winterson
Publikováno v:
Angewandte Chemie International Edition. 58:9811-9815
An efficient and reliable electrochemical generator of hypervalent iodine reagents has been developed. In the anodic oxidation of iodoarenes to hypervalent iodine reagents under flow conditions, the use of electricity replaces hazardous and costly ch
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::5dd719652e0f646e73468d2d87914cda
https://doi.org/10.1002/anie.201904379
https://doi.org/10.1002/anie.201904379
Autor:
Célina Génot, Bethan Winterson, Mohamed Elsherbini, Thomas Wirth, Haifa Alharbi, Ana A. Folgueiras-Amador
Publikováno v:
Angewandte Chemie. 131:9916-9920
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_________::e94716000ef91290f8e84d275a7c959d
https://doi.org/10.1002/ange.201904379
https://doi.org/10.1002/ange.201904379
Autor:
Oscar de Frutos, Stephen J. Pickering, Derek Pletcher, Carlos Mateos, Medhat Sharabi, Katie E. Jolley, Ana A. Folgueiras-Amador, Peter R. Birkin, Juan A. Rincón, Richard C. D. Brown
Publikováno v:
Electrochemistry Communications, Vol 100, Iss, Pp 6-10 (2019)
It is demonstrated that the addition of a non-ionic surfactant (Triton X-100 or Brij L23) to the electrolyte medium leads to a significant improvement to the current efficiency for the methoxylation of N-formylpyrrolidine in a flow electrolysis cell
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::49199892c811cf9dfbee1b0da952c631
http://www.sciencedirect.com/science/article/pii/S1388248119300098
http://www.sciencedirect.com/science/article/pii/S1388248119300098
Despite extensive literature on organic electrosynthesis, it has never become a routine procedure in organic synthesis laboratories. One reason is certainly a lack of attention to the design of the cell used for the electrolysis; an appropriate cell
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::4ea70c42f3a6867c72d9463dc14bee37
https://eprints.soton.ac.uk/438361/
https://eprints.soton.ac.uk/438361/
Publikováno v:
Chemistry - A European Journal. 24:487-491
A catalyst- and supporting electrolyte-free method for\ud electrochemical dehydrogenative C–S bond formation in continuous\ud flow has been developed. A broad range of N‑ arylthioamides have\ud been converted to the corresponding benzothiazoles i
Externí odkaz:
https://explore.openaire.eu/search/publication?articleId=doi_dedup___::1c6ffeabada1675ddf9ded1ae6945612
https://doi.org/10.1002/chem.201705016
https://doi.org/10.1002/chem.201705016