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Visible Light-Induced, Nickel-Catalyzed Late-Stage 4-Alkylation of Hantzsch Esters with Alkyl Bromide.

Autor: Yan-Ling Liu, Xian-Chen He, Jie Gao, Ke-Rong Li, Kai Chen, Hao-Yue Xiang, Hua Yang

Publikováno v: Journal of Organic Chemistry; 8/2/2024, Vol. 89 Issue 15, p10987-10997, 11p

Novel biologically active paddlewheel-like palladium thiocyanate complex catalyzed cyanation of alkyl bromide utilizing Q-tube system: A green perspective

Autor: El-bendary, Mohamed M., Akhdhar, Abdullah, Saleh, Tamer S.

Publikováno v: In Polyhedron 1 April 2024 252

Giese-type alkylation of dehydroalanine derivatives via silane-mediated alkyl bromide activation.

Autor: van der Heide P; Department of Chemical and Geological Sciences, University of Cagliari, S.S. 554, bivio per Sestu, 09042 Monserrato (CA), Italy.; Flow Chemistry Group, Van 't Hoff Institute for Molecular Sciences (HIMS), University of Amsterdam Science Park 904, 1098 XH Amsterdam, The Netherlands., Retini M; Department of Biomolecular Sciences, University of Urbino ''Carlo Bo', Piazza Rinascimento 6, 61029 Urbino, Italy., Fanini F; Department of Biomolecular Sciences, University of Urbino ''Carlo Bo', Piazza Rinascimento 6, 61029 Urbino, Italy., Piersanti G; Department of Biomolecular Sciences, University of Urbino ''Carlo Bo', Piazza Rinascimento 6, 61029 Urbino, Italy., Secci F; Department of Chemical and Geological Sciences, University of Cagliari, S.S. 554, bivio per Sestu, 09042 Monserrato (CA), Italy., Mazzarella D; Department of Chemical Sciences and Technologies, University of Rome 'Tor Vergata' Via della Ricerca Scientifica, 1, 00133 Rome, Italy.; Department of Chemical Sciences, University of Padova Institution, Via Francesco Marzolo, 1, 35131 Padova, Italy., Noël T; Flow Chemistry Group, Van 't Hoff Institute for Molecular Sciences (HIMS), University of Amsterdam Science Park 904, 1098 XH Amsterdam, The Netherlands., Luridiana A; Department of Chemical and Geological Sciences, University of Cagliari, S.S. 554, bivio per Sestu, 09042 Monserrato (CA), Italy.

Publikováno v: Beilstein journal of organic chemistry [Beilstein J Org Chem] 2024 Dec 17; Vol. 20, pp. 3274-3280. Date of Electronic Publication: 2024 Dec 17 (Print Publication: 2024).

Analyzing Alkyl Bromide Genotoxic Impurities in Febuxostat Based on Static Headspace Sampling and GC-ECD

Autor: Alexandros Kavrentzos, Elli Vastardi, Evangelos Karavas, Paraskevas D. Tzanavaras, Constantinos K. Zacharis

Publikováno v: Pharmaceuticals, Vol 17, Iss 4, p 422 (2024)

Herein, a sensitive and selective gas chromatography-electron capture detector (GC-ECD) method was developed and validated for the quantification of trace levels of five bromo-containing genotoxic impurities in Febuxostat active pharmaceutical ingred

Externí odkaz: https://doaj.org/article/ee4b5c9228e64a4db145711a4897533a