Zobrazeno 1 - 10
of 16
pro vyhledávání: '"Adam D. Raw"'
Autor:
Adam D. Raw, James A. Ibers
Publikováno v:
Acta Crystallographica Section E, Vol 67, Iss 12, Pp i70-i70 (2011)
Zirconium(IV) dilanthanum(III) pentasulfide, ZrLa2S5, crystallizes with four formula units in the space group Pnma in the U3S5 structure type. The asymmetric unit comprises one Zr, one La and four S atoms. The Zr and three S atoms are situated on mir
Externí odkaz:
https://doaj.org/article/6a70a1023d964369b91908ce0bff1fd5
Publikováno v:
Journal of Solid State Chemistry. 200:165-169
A novel method involving a molten Ga flux for the synthesis of diffraction quality crystals of the compound Cu{sub 3.82(1)}Mo{sub 3}O{sub 12}, a copper molybdate in the Lyonsite (α-Cu{sub 3}Fe{sub 4}(VO{sub 4}){sub 6}) family, has been developed. Si
Autor:
Adam D. Raw, David S. Ginley, Arthur J Freeman, Giancarlo Trimarchi, Thomas O. Mason, Andriy Zakutayev, Veerle Cloet, Nicola H. Perry, Haowei Peng, John D. Perkins, Jino Im, Paul F. Ndione, Kenneth R. Poeppelmeier
Publikováno v:
Chemistry of Materials. 24:3346-3354
The structures of α- and β-Ag3VO4 were studied via single- crystal X-ray diffraction (XRD). The transition from α-phase to β-phase was found to occur at 110 °C. Single-crystal XRD revealed that the integrity of the single crystals was maintained
Publikováno v:
Journal of Solid State Chemistry. 192:34-37
During reinvestigation of the hydrothermal synthesis reported earlier of the compound cesium nickel phosphide, “CsNiP”, we arrived at a new route to the synthesis of the cesium nickel halide compounds CsNiX 3 (X=Cl, Br, I). The method has also be
Autor:
Adam D. Raw, James A. Ibers
Publikováno v:
Journal of Solid State Chemistry. 187:282-285
Black square plates of the new compound UEr2O2S3 have been synthesized by the reaction of UOS, Er, and S with an Sb2S3 flux at 1273 K. The structure of UEr2O2S3 has been solved and refined from single-crystal X-ray diffraction data. UEr2O2S3 forms a
Autor:
Adam D. Raw, James A. Ibers
Publikováno v:
Journal of Solid State Chemistry. 186:177-181
Single crystals of the new uranium lanthanide oxyselenide compounds UYb{sub 2}O{sub 2}Se{sub 3} and U{sub 2}Ln{sub 2}O{sub 4}Se{sub 3} (Ln=Pr, Sm, Gd) have been synthesized from an Sb{sub 2}Se{sub 3} flux. The structures have been determined from sin
Autor:
Suntharalingam Skanthakumar, Geng Bang Jin, L. Soderholm, Richard G. Haire, Adam D. Raw, James A. Ibers
Publikováno v:
Journal of Solid State Chemistry. 183:547-550
The compounds UOS, UOSe, NpOS, and NpOSe have been synthesized and their structures determined by means of single-crystal X-ray diffraction methods. The results provide more detailed crystallographic information, including more precise interatomic di
Publikováno v:
ChemInform. 44
Polycrystalline, diffraction quality powders of Cu3.82Mo3O12 are obtained by solid state reaction of stoichiometric amounts of Cu2O, CuO, and MoO3 (fused silica tube, 803 K, 2 d, slow cooling) followed by treatment of the resulting powder in a Ga flu
Publikováno v:
ChemInform. 43
Single crystals of the title compounds are prepared by hydrothermal reaction of NiX2 (X: Cl, Br, I), CsOH, and 85% aq.
Autor:
James A. Ibers, Adam D. Raw
Publikováno v:
ChemInform. 43
Single crystals of UEr2O2S3 in the form of large black square plates are prepared by solid state reaction of UOS, Er, S, and Sb2S3 as a flux (1273 K, 14 d, 30 wt.% yield).