Zobrazeno 1 - 10
of 60
pro vyhledávání: '"A. J. PERROTTA"'
Publikováno v:
Microporous and Mesoporous Materials. 153:18-23
Single crystals of a three dimensional ammonium aluminophosphate (PSU-3) have been synthesized as a minor phase in the synthesis of the unknown cyclohexylamine templated ALPO structure UHM-5, and its structure determined by single crystal X-ray diffr
Publikováno v:
Microporous and Mesoporous Materials. 123:274-279
Single crystals of hexagonal and dihexagonal morphology cancrinites, crystallized in the same batch reaction with sodalite, have been characterized by X-ray diffraction analysis. Although the unit cell values are almost identical, Si–O bond lengths
Publikováno v:
Crystal Growth & Design. 6:2072-2075
Large transparent crystals (up to 800 μm) of a hydroxy-sodium gallogermanate sodalite have been prepared at between 100 and 150 °C in aqueous sodium tetramethylammonium hydroxide solutions. Single-crystal structure analysis gave the expected space
Publikováno v:
Chemistry of Materials. 18:3611-3615
By reacting a pre-made aluminophosphate (ALPO, P:Al = 0.9) gel with an aqueous tripropylamine solution of KOH and TMAOH, we have synthesized a new porous 3D crystalline structure (PSU-2) under high...
Autor:
Gregory S. Rohrer, Anthony J. Perrotta, Neal R. Dando, Altaf H. Carim, Shih-Ying Tzeng, Cathy Lane Rohrer
Publikováno v:
Journal of the American Ceramic Society. 80:2677-2680
A new two-step transformation sequence has been identified for the conversion of diaspore (α-AlOOH) to corundum (alpha-Al2O3). The powder X-ray diffraction pattern of the intermediate phase, designated alpha'-Al2O3, has been indexed to a monoclinic
Publikováno v:
Journal of the American Ceramic Society. 84:1896-1902
“Diasporic” precursors derived from sols formed by the controlled hydrolysis of aluminum sec-butoxide in the presence of HCl yielded mixtures of corundum and amorphous alumina when calcined between 500° and 800°C. The fraction of corundum in th
Publikováno v:
Journal of the American Ceramic Society. 85:2325-2330
The influence of magnesium, phosphorus, and iron additions on the low-temperature (≤1000°C) sintering of nanocrystalline α-Al 2 O 3 derived from α-AlOOH has been investigated. α-AlOOH powder with a surface area of 50 m 2 /g yielded α-Al 2 O 3
Publikováno v:
Journal of Dispersion Science and Technology. 22:143-165
Direct precipitation of metal oxides from high boiling point organic solvents presents an alternative to wholly aqueous hydrothermal material synthesis routes. In the current study, reaction conditions to control particle size and shape of α-alumina
Autor:
Yimei Zhu, Shigeo Ohshio, Yacov Haimes, Wei Huang, Yanchun Zhou, Hans Conrad, Hirotaka Wakabayashi, Hidetoshi Saitoh, Yoshiaki Takata, Xiaochun Wu, Li Wang, Rongyao Wang, Norio Tanaka, Bingsuo Zou, Sishen Xie, S. Shimomsto, Qianwang Chen, A. J. Perrotta, Jay Switzer, Jiren Xu, Li Fei, Noriyuki Yamasaki, Keizo Uematsu
Publikováno v:
Materials Technology. 13:80-83
Publikováno v:
Science. 277:788-791
Corundum, α-Al 2 O 3 , is the thermodynamically stable phase of coarsely crystalline aluminum oxide, but syntheses of nanocrystalline Al 2 O 3 usually result in γ-Al 2 O 3 . Adsorption microcalorimetry, thermogravimetric analyses, and Brunauer-Emme