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Publikováno v:
CCS Chemistry. 4:855-863
The first postsynthetic solution-based crystal transformation of two-dimensional metal halide perovskites (2D MHPs) through organothiol-based reactions is reported. It is well-established that the ...
Publikováno v:
Chemistry – An Asian Journal. 16:2118-2125
The intramolecularly double-donor-stabilized stannylene 1 has been synthesized from the salt-metathesis reaction between two equivalents of lithium pyridine ene-amide L1 and SnCl2 . Compound 1 exhibits dipolar behavior when reacted with B(C6 F5 )3 le
Publikováno v:
Angewandte Chemie (International Ed. in English)
130 years after Mond discovered the first homoleptic carbonyl complex Ni(CO)4, we report on a [Ni(CO)4].+ salt as the first synthesis of any homoleptic nickel carbonyl cation in the condensed phase. It was prepared by oxidation of nickel metal with t
Publikováno v:
Crystallography Reports. 66:461-467
Two metal coordination polymers, namely {[Ni(H2O)2(1,3-BIP)2] ⋅ TFBDC}n (I), {[Cu3(H2O)4(1,3-BIP)6] ⋅ (BTC)2 ⋅ (H2O)15}n (II), (1,3-BIP is 1,3-bis(imidazole)propane, H2TFBDC is 2,3,5,6-tetrafluoroterephthalic acid and H3BTC is 1,3,5-benzenetric
Publikováno v:
Angewandte Chemie. 133:11531-11536
Silver nanoclusters containing Ag0 atoms protected by amino acids were synthesized and characterized. Chiral superatomic silver nanoclusters [Ag47 L12 (C≡Ct Bu)16 ]BF4 (L=l-/d-valine or l-/d-isoleucine) have been prepared by reducing AgC≡Ct Bu an
Autor:
Carsten von Hänisch, Fabian Dankert, Markus Balmer, Xiulan Xie, Roman-Malte Richter, Florian Weigend
Publikováno v:
Angewandte Chemie (International Ed. in English)
We herein report the synthesis, structures, coordination ability, and mechanism of formation of silicon analogs of crown ethers. An oligomerization of 2D2 (I) (2Dn,=(Me4Si2O)n) was achieved by the reaction with GaI3 and MIx (M=Li, Na, Mg, Ca, Sr). In
Autor:
Timothy R. Wagner, Oscar Kipruto Keino
Publikováno v:
Journal of Chemical Crystallography. 51:536-542
A new Group 2 bimetallic nitride fluoride phase of approximate composition SrCaNF has been prepared and characterized via high resolution single crystal X-ray diffraction. Single crystalline samples were prepared from reaction of SrF2 with Ca and Sr
Publikováno v:
CrystEngComm. 23:569-590
Three new amine functionalised tetracarboxylate linkers with a variety of arm lengths were synthesised, namely N,N,N′N′-tetrakis(R1, R2 or R3)-trans-1,4-diaminocyclohexane, R1 = (4-carboxyphenyl)-1-methyl; R2 = (4-cinnamic)-1-methyl; R3 = 1′-ca
Autor:
Baishakhi Pal, Akhtaruzzaman, Partha Pratim Ray, Suvendu Maity, Mohammad Hedayetullah Mir, Sanobar Naaz, Samim Khan, Prasanta Ghosh, Basudeb Dutta
Publikováno v:
CrystEngComm. 23:7525-7533
A new Cd(II)-based two-dimensional coordination polymer (2D CP) [{Cd2(cis-1,4-chdc)2(1,10-phen)2}·5H2O]n (1) has been synthesized at room temperature by a slow diffusion technique using a 1,4-cyclohexanedicarboxylic acid (1,4-H2chdc) and 1,10-phenan
Publikováno v:
CrystEngComm. 23:3160-3166
The treatment of the metal sulfide precursor [Et4N][Tp*WS3] (Tp* = hydridotris(3,5-dimethylpyrazol-1-yl)borate) (1) with Cu(I) and the Fe-bipyridine complex ligand L1 in the presence of (NH4)2SO4 produced one-dimensional (1D) [(Tp*WS3Cu2)2(L1)2](BF4)