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Publikováno v:
Journal of Chromatographic Science. 59:458-464
Rufinamide (RF), antiepileptic drug, is biotransformed to inactive metabolite. Frequent plasma monitoring is required for dose adjustment. This work is concerned with the development and validation of a sensitive and selective RP-HPLC method for the
Publikováno v:
Journal of Chromatographic Science. 59:371-380
Herbals that are widely consumed as therapeutic alternatives to conventional drugs for cardiovascular diseases, may lead to herb–drug interactions (HDIs). Atorvastatin (ATR) is drug of choice for hyperlipidemia and is extensively metabolized throug
Publikováno v:
Journal of Chromatographic Science. 59:419-424
A simple and reliable HPLC method is developed for isocratic separation of a ternary mixture of Salbutamol Sulfate (SAL), Guaifenesin (GUI) and its impurity Guaiacol (GUA) either in pure powder or in pharmaceutical formulation. Chromatographic separa
Publikováno v:
Journal of Chromatographic Science. 59:338-346
A simple and reliable high-performance liquid chromatography method for simultaneous quantitation of gliclazide and ciprofloxacin in plasma sample has been developed and validated. This method implements protein precipitation, a simple and practical
Autor:
Felix Maurer, Heinrich Groesdonk, Tobias Hüppe, Thomas Volk, Beate Wolf, Daniel I. Sessler, Teodora Shopova, Sascha Kreuer
Publikováno v:
Journal of Chromatographic Science. 59:165-174
Fosfomycin is an antibiotic with a broad spectrum of activity against many multidrug-resistant bacterial strains. It is mainly excreted unchanged by the kidneys, and its half-life therefore depends on kidney function which varies considerably among i
Publikováno v:
Journal of Chromatographic Science. 59:112-119
A new, simple and stability-indicating gas chromatography-flame ionization detection (GC-FID) method was developed and validated for the quantitative determination of busulfan and its organic impurities (OI) in drug substance without derivatization.
Publikováno v:
Journal of Chromatographic Science. 59:217-222
An ion chromatography (IC) system with switching recycling column was developed for the determination of bromate in drinking water with high chloride content. The system included a pump, two switching valves, guard column and analytical column, suppr
Publikováno v:
Journal of Chromatographic Science. 58:907-914
Dipeptidyl peptidase-4 inhibitors, so-called gliptins, constitute a fairly novel class of oral hypoglycemic agents. The development and validation of an automated online SPE-LC-UV method to determine intact sitagliptin, saxagliptin, vildagliptin and
Publikováno v:
Journal of Chromatographic Science. 58:880-886
An environmentally friendly method for the determination of testosterone and methyltestosterone by acid–base-induced deep eutectic solvents liquid–liquid microextraction (DES-ABLLME) combining with high-performance liquid chromatography was estab
Publikováno v:
Journal of Chromatographic Science. 58:622-628
Accurate, rapid and selective reversed phase ultra-performance liquid chromatography method with UV detection has been established and validated for the synchronous determination of aceclofenac (ACE) and diacerin (DIA) in the occurrence of diclofenac